Quadrupole mass spectrometry and optical emission spectroscopy: detection capabilities and representative sampling of short transient signals from laser-ablation

2000 ◽  
Vol 15 (9) ◽  
pp. 1149-1155 ◽  
Author(s):  
Thomas Pettke ◽  
Christoph A. Heinrich ◽  
Adeline C. Ciocan ◽  
Detlef Günther
Keyword(s):  
Mass Spectrometry ◽  
Laser Ablation ◽  
Emission Spectroscopy ◽  
Optical Emission Spectroscopy ◽  
Optical Emission ◽  
Quadrupole Mass ◽  
Transient Signals ◽  
Representative Sampling ◽  
Quadrupole Mass Spectrometry ◽  
Detection Capabilities

Characterization of two modes in a dielectric barrier discharge probe by optical emission spectroscopy and time-of-flight mass spectrometry

2015 ◽  
Vol 30 (12) ◽  
pp. 2496-2506 ◽  
Author(s):  
Andreas Bierstedt ◽  
Ulrich Panne ◽  
Knut Rurack ◽  
Jens Riedel
Keyword(s):  
Mass Spectrometry ◽  
Dielectric Barrier Discharge ◽  
Emission Spectroscopy ◽  
Optical Emission Spectroscopy ◽  
Barrier Discharge ◽  
Optical Emission ◽  
Dielectric Barrier ◽  
Flight Mass Spectrometry ◽  
Individual Product

A dielectric barrier discharge probe has been developed, which enables switching between two individual product channels yielding either protonated or ammoniated molecules.

scholarly journals Coloring hot-dip galvanization of steel samples in industrial zinc-manganese baths

2017 ◽  
Vol 53 (3) ◽  
pp. 319-326 ◽  
Author(s):  
M. Godzsák ◽  
G. Lévai ◽  
K. Vad ◽  
A. Csik ◽  
J. Hakl ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Glow Discharge ◽  
Wall Thickness ◽  
Emission Spectroscopy ◽  
Optical Emission Spectroscopy ◽  
Optical Emission ◽  
Chemical Thermodynamics ◽  
Light Interference ◽  
Mn Content ◽  
Galvanized Coating

Colored hot dip galvanization of various steel samples was realized in an industrial bath containing 738 kg of a Zn-Mn liquid alloy at 450?C. Zinc was alloyed in three steps to reach 0.1, 0.15 and 0.2 w% of Mn in liquid zinc, and galvanization of 9 different steel samples was performed in all three baths. The obtained colors change in the sequence blue - yellow - pink - green with increasing the Mn-content of the bath and with increasing the wall thickness of the steel samples. The results are analyzed by Glow-discharge optical emission spectroscopy (GD-OES) and Secondary Neutral Mass Spectrometry (SNMS) techniques. It is shown that depending on the Mn-content and on the wall thickness of the steel the samples are coated by MnO of various thicknesses (in the range between 30 - 230 nm). This layer forms when the samples are removed from the Zn-Mn bath into surrounding air, before the Zn-layer is solidified. Light interference on this thin MnO layer causes the colors of the galvanized coating. Different colors are obtained in different ranges of MnO thicknesses, in accordance with the laws of optics. The minimum Mn-content of liquid Zn is found as 0.025 ? 0.010 m/m% to ensure that the original outer ZnO layer on Zn is converted into the MnO layer. This minimum critical Mn-content is in agreement with chemical thermodynamics.

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