Application of gas-liquid chromatography to the analysis of essential oils. Part VII. Fingerprinting of essential oils by temperature-programmed gas-liquid chromatography using a carbowax 20M stationary phase

The Analyst ◽  
1980 ◽  
Vol 105 (1248) ◽  
pp. 262 ◽  
Keyword(s):  
Liquid Chromatography ◽  
Stationary Phase ◽  
Essential Oils ◽  
Gas Liquid Chromatography ◽  
Temperature Programmed

Quantitation of anticonvulsant drugs in serum by gas-chromatography on the stationary phase SP-2510.

1978 ◽  
Vol 24 (3) ◽  
pp. 483-485 ◽  
Author(s):  
W Godolphin ◽  
J Thoma
Keyword(s):  
Gas Chromatography ◽  
Liquid Chromatography ◽  
Stationary Phase ◽  
Serum Cholesterol ◽  
Anticonvulsant Drugs ◽  
Gas Liquid Chromatography ◽  
Column Packing ◽  
Extraction Procedures

Abstract A new column packing, SP-2510 DA (Supelco, Inc., Bellefonte, Pa. 16823), is an excellent stationary phase for the determination of a wide variety of anticonvulsant drugs by gas--liquid chromatography without derivatization. However, when uncomplicated extraction procedures are used, serum cholesterol interferes with the determination of primidone. By the simple expedient of adding a short "pre-column" containing another phase (SP-2250 DA) the problem is overcome.

Simultaneous Determination of Urinary Estriol, Pregnanediol, and Pregnanolone by Gas-Liquid Chromatography

1969 ◽  
Vol 15 (3) ◽  
pp. 190-196 ◽  
Author(s):  
Robert D Baynton ◽  
Donald J Campbell
Keyword(s):  
Liquid Chromatography ◽  
Glycol Succinate ◽  
Urine Specimen ◽  
Gas Liquid Chromatography ◽  
Large Hospital ◽  
Flame Ionization ◽  
Trimethylsilyl Ethers ◽  
Hydrogen Flame ◽  
Progesterone Metabolites ◽  
Temperature Programmed

Abstract A simplified method for following the urinary excretion of estriol, pregnanediol, and pregnanolone during the course of pregnancy is presented. The procedure has been used successfully in a large hospital laboratory. An important advantage is that the estrogen and progesterone metabolites are measured simultaneously, and separate extraction and gas-liquid chromatography is not required. The urine specimen is hydrolyzed enzymatically, extracted, and the steroids are converted to trimethylsilyl ethers. Temperature-programmed gas-liquid chromatography is carried out on a 2% neopentyl glycol succinate column using a hydrogen flame ionization detector.

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