The determination of non-fat milk solids in milk bread from the orotic acid content

The Analyst ◽  
1973 ◽  
Vol 98 (1171) ◽  
pp. 755 ◽  
Author(s):  
A. W. Archer
Keyword(s):  
1989 ◽  
Vol 72 (4) ◽  
pp. 627-631
Author(s):  
Lap V Bui

Abstract A sensitive and reproducible isocratic liquid chromatographic method is described for the determination of orotic acid levels in skim milk powder and milk bread. The results are used to calculate the nonfat milk solids content in milk bread. Sample preparation is simple and rapid and produces an extract which, after passing through an on-line cleanup system, has a minimum adverse effect on the performance and life of the analytical column. Mean recoveries of 96-105% were obtained with coefficients of variation in the range 1.0-8.5% and a detection limit of 5 mg/kg. The liquid chromatographic method was more sensitive than the standard colorimetric method, while results obtained by both methods agreed closely.


1957 ◽  
Vol 12 (2) ◽  
pp. 125-129 ◽  
Author(s):  
Nobuyasu KAWASAKI ◽  
Ichiro TAKI ◽  
Chiaki WATANABE ◽  
Kiyoshi MATOBA ◽  
Mokichiro NISHIO ◽  
...  

2016 ◽  
Vol 2 (1) ◽  
pp. 37-42 ◽  
Author(s):  
J.M. Pino Moreno ◽  
A. Ganguly

In the present paper we have determined the fatty acid content of some edible insects of Mexico. A comparative analysis of the insect species studied in this research showed that caproic acid was present in a minimal proportion which ranged between 0.01 for Periplaneta americana (nymphs) and 0.06 (g/100 g, dry basis) for Euschistus strenuus. The highest proportion of caprilic acid (0.09) was found in Tenebrio molitor (adults). Atta sp. had the highest amount of capric acid (0.26). Polistes sp. was found to be rich in lauric acid (0.77) and for myristic acid it had the highest content (5.64). Dactylopius sp. and E. strenuus were rich in palmitic acid (14.89). Euschistus taxcoensis had the highest quantity of palmitoleic acid (12.06). Llaveia axin exhibited the highest quantity of stearic acid (22.75). Polistes sp. was found to be rich in oleic acid (38.28). The highest quantity of linoleic acid was observed in T. molitor (larvae) (10.89), and in L. axin the highest content of linolenic acid (7.82) was obtained. A comparison between the species under the present investigation revealed that, in general, the insects are poor in caproic, caprilic, capric, lauric, myristic, palmitoleic and linolenic acids, because the quantities were either minimal or could not be detected at all. They had moderate quantities of stearic, palmitic and linoleic acids and had high quantities of oleic acid. Finally it was concluded that although a particular insect species is unable to fulfil the total fatty acid need for a human, if consumed in combination they could definitely be able to supply a good amount of this highly valued nutrient.


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