The volumetric determination of uranium after reduction by lead in dilute perchloric acid solution

The Analyst ◽  
1960 ◽  
Vol 85 (1006) ◽  
pp. 55 ◽  
Author(s):  
T. W. Steele
Keyword(s):  
Acid Solution ◽  
Perchloric Acid ◽  
Perchloric Acid Solution ◽  
Volumetric Determination

A Simplified Technique for Determination of Small Amounts of Calcium as Oxalate

1964 ◽  
Vol 10 (4) ◽  
pp. 352-365
Author(s):  
Donald D Van Slyke ◽  
Paul E Carson
Keyword(s):  
Acid Solution ◽  
Calcium Oxalate ◽  
Perchloric Acid ◽  
Perchloric Acid Solution ◽  
Ceric Sulfate ◽  
Glass Filter ◽  
Oxalate Precipitation ◽  
Oxalate Solution ◽  
Filter Tube

Abstract Procedures for determination of calcium by oxalate precipitation are reviewed, and a method is described in which the calcium oxalate precipitate is both formed and washed in a filter tube with a fritted-glass filter. Washing with saturated calcium oxalate solution is completed in 1-2 min. The washed precipitate is redissolved in perchloric acid solution and the dissolved oxalate is either titrated or determined manometrically by the CO2 evolved from oxidation with ceric sulfate.

Extended Preservation of Iron for Transmission

1967 ◽  
Vol 25 ◽  
pp. 354-355
Author(s):  
E. P. Abrahamson II ◽  
M. W. Dumais
Keyword(s):  
Acid Solution ◽  
Perchloric Acid ◽  
Microscopy Study ◽  
Perchloric Acid Solution ◽  
Transmission Microscopy ◽  
Iron Base ◽  
Cold Stage

In a transmission microscopy study of iron and dilute iron base alloys, it was determined that it is possible to preserve specimens for extended periods of time. Our specimens were prepunched from 5 to 8 mil sheet to microscope size and annealed for several hours at 700°C. They were then thinned in a glacial acetic-12 percent perchloric acid solution using 10 volts and 20 milliamperes, at a temperature of 8 to 14°C.It was noted that by the use of a cold stage, the same specimen can be observed for periods up to one week without excess contamination. When removal of the specimen from the column becomes necessary, it was observed that a specimen may be kept for later observation in 1,2 dichloroethene or methanol for periods in excess of two weeks.

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