Ultrasonic extraction and colorimetric determination of anionic surfactants in marine sediments by the ethyl violet method

1996 ◽  
Vol 33 (9) ◽  
pp. 303 ◽  
Author(s):  
Mauro Mecozzi ◽  
Marina Amici ◽  
Eva Pietrantonio
1982 ◽  
Vol 54 (3) ◽  
pp. 392-397 ◽  
Author(s):  
Shoji. Motomizu ◽  
Sigeru. Fujiwara ◽  
Akihiro. Fujiwara ◽  
Kyoji. Toei

2011 ◽  
Vol 6 (No. 4) ◽  
pp. 198-204 ◽  
Author(s):  
L. Yu ◽  
M. Wu ◽  
W. Dong ◽  
J. Jin ◽  
X. Zhang

  In order to control the pollution by anionic surfactants in seawater, a simple, accurate and sensitive reverse flow injection (rFIA) spectrophotometric method for the determination of anionic surfactants in seawater is suggested in this paper. Sodium dodecylbenzenesulfonate (LAS) was selected as the reference anionic surfactant. The method is based on the ion associate formed between LAS and Ethyl Violet. The absorbance of the complex is measured by optical detector at 585 nm. Chemical factors and rFIA variables affecting the system are also discussed. Under the optimal conditions, the linear range of this method was 25.0–400.0 μg/l; the detection limit was 2.4 μg/l; the relative standard deviation was 0.38%. This method is suitable for automatic and continuous analysis, and was successfully applied to determine the content of anionic surfactants in seawater.


1959 ◽  
Vol 36 (2) ◽  
pp. 193-201 ◽  
Author(s):  
Julius A. Goldbarg ◽  
Esteban P. Pineda ◽  
Benjamin M. Banks ◽  
Alexander M. Rutenburg

2013 ◽  
Vol 12 (7) ◽  
pp. 460-465
Author(s):  
Sameer Amereih ◽  
Zaher Barghouthi ◽  
Lamees Majjiad

A sensitive colorimetric determination of fluoride in drinking water has been developed using a polymeric zirconium complex of 5-(2-Carboxyphenylazo)-8-Hydroxyquinoline as fluoride reagents. The method allowed a reliable determination of fluoride in range of (0.0-1.5) mg L-1. The molar absorptivity of the complex formation is 7695 ± 27 L mol-1 cm-1 at 460 nm. The sensitivity, detection limit, quantitation limit, and percentage recovery for 1.0 mg L-1 fluoride for the proposed method were found to be 0.353 ± 0.013 μg mL-1, 0.1 mg L-1, 0.3 mg L-1, and 101.7 ± 4.1, respectively.


Author(s):  
Abbas Shebeeb Al-kadumi ◽  
Sahar Rihan Fadhel ◽  
Mohammed Abdullah Ahmed ◽  
Luma Amer Musa

We proposed two simple, rapid, and convenient spectrophotometric methods are described for the determination of Amoxicillin in bulk and its pharmaceutical preparations. They are based on the measurement of the flame atomic emission of potassium ion (in first method) and colorimetric determination of the green colored solution for manganite ion at 610 nm formed after reaction of Amoxicillin with potassium permanganate as oxidant agent (in the second method) in basic medium. The working conditions of the methods were investigated and optimized. Beer's law plot showed a good correlation in the concentration range of 5-45 μg/ml. The detection limits and relative standared deviations were (2.573, 2.814 μg/ml) (2.137, 2.498) for the flame emission photometric method and (1.844, 2.016 μg/ml) (1.645,1.932) for colorimetric methods for capsules and suspensions respectively. The methods were successfully applied to the determination of Amoxicillin in capsules and suspensions, and the obtained results were in good agreement with the label claim. No interference was observed from the commonly encountered additives and expectancies.


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