Novel Fluorination of Small-ring Tertiary Cycloalkanols: Reaction of Diethylaminosulfur Trifluoride with Tertiary Cyclobutanols

1998 ◽  
pp. 652-653 ◽  
Author(s):  
Masayuki Kirihara ◽  
Tomofumi Takuwa ◽  
Toshihiro Kambayashi ◽  
Takefumi Momose ◽  
Yoshio Takeuchi
ChemInform ◽  
2010 ◽  
Vol 30 (15) ◽  
pp. no-no
Author(s):  
Masayuki Kirihara ◽  
Tomofumi Takuwa ◽  
Toshihiro Kambayashi ◽  
Takefumi Momose ◽  
Yoshio Takeuchi

2001 ◽  
Author(s):  
G. Maas ◽  
K.-P. Zeller ◽  
N. Tokitoh ◽  
W. Ando ◽  
H. Heydt ◽  
...  
Keyword(s):  

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Daniel Gomes da Silva Machado ◽  
Marom Bikson ◽  
Abhishek Datta ◽  
Egas Caparelli-Dáquer ◽  
Gozde Unal ◽  
...  

AbstractTranscranial direct current stimulation (tDCS) has been used aiming to boost exercise performance and inconsistent findings have been reported. One possible explanation is related to the limitations of the so-called “conventional” tDCS, which uses large rectangular electrodes, resulting in a diffuse electric field. A new tDCS technique called high-definition tDCS (HD-tDCS) has been recently developed. HD-tDCS uses small ring electrodes and produces improved focality and greater magnitude of its aftereffects. This study tested whether HD-tDCS would improve exercise performance to a greater extent than conventional tDCS. Twelve endurance athletes (29.4 ± 7.3 years; 60.15 ± 5.09 ml kg−1 min−1) were enrolled in this single-center, randomized, crossover, and sham-controlled trial. To test reliability, participants performed two time to exhaustion (TTE) tests (control conditions) on a cycle simulator with 80% of peak power until volitional exhaustion. Next, they randomly received HD-tDCS (2.4 mA), conventional (2.0 mA), or active sham tDCS (2.0 mA) over the motor cortex for 20-min before performing the TTE test. TTE, heart rate (HR), associative thoughts, peripheral (lower limbs), and whole-body ratings of perceived exertion (RPE) were recorded every minute. Outcome measures were reliable. There was no difference in TTE between HD-tDCS (853.1 ± 288.6 s), simulated conventional (827.8 ± 278.7 s), sham (794.3 ± 271.2 s), or control conditions (TTE1 = 751.1 ± 261.6 s or TTE2 = 770.8 ± 250.6 s) [F(1.95; 21.4) = 1.537; P = 0.24; η2p = 0.123]. There was no effect on peripheral or whole-body RPE and associative thoughts (P > 0.05). No serious adverse effect was reported. A single session of neither HD-tDCS nor conventional tDCS changed exercise performance and psychophysiological responses in athletes, suggesting that a ceiling effect may exist.


2020 ◽  
Vol 2020 ◽  
pp. 1-12
Author(s):  
Xiaoqin Hao ◽  
Jia Yu ◽  
Weidong He ◽  
Yi Jiang

To solve the problem of the effective cushioning of fast-moving mechanical components in small ring-shaped spaces, the factors affecting the compression and energy absorption properties of small-sized hollow metal tubes were studied. Simulation models were constructed to analyse the influences of tube diameter, wall thickness, relative position, and number of stacked components on the compression and energy absorption properties. The correctness of the simulation method and its output were verified by experiments, which proved the effectiveness of compression and energy absorption properties of small-sized thin-walled metal tubes. The research provides support for the application of metal tube buffers in armament launch technology and engineering practice.


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