A Novel Chiral Resolving Reagent, Bis((S)-Mandelic acid)-3-nitrophthalate, for Amlodipine Racemate Resolution: Scalable Synthesis and Resolution Process

2009 ◽  
Vol 13 (6) ◽  
pp. 1382-1386 ◽  
Author(s):  
Hong Woo Lee ◽  
Sung Jae Shin ◽  
Hosung Yu ◽  
Sung Kwon Kang ◽  
Choong Leol Yoo
Keyword(s):  
Mandelic Acid ◽  
Racemate Resolution ◽  
Resolution Process ◽  
Scalable Synthesis

An Efficient and Scalable Synthesis of the Endothelin Antagonists UK-350,926 and UK-349,862 Using a Dynamic Resolution Process

2005 ◽  
Vol 9 (5) ◽  
pp. 663-669 ◽  
Author(s):  
Christopher P. Ashcroft ◽  
Stephen Challenger ◽  
David Clifford ◽  
Andrew M. Derrick ◽  
Yousef Hajikarimian ◽  
...  
Keyword(s):  
Resolution Process ◽  
Endothelin Antagonists ◽  
Dynamic Resolution ◽  
Scalable Synthesis

Differential Effects of Prior Experience on the Malware Resolution Process

MIS Quarterly ◽  
2014 ◽  
Vol 38 (3) ◽  
pp. 655-678 ◽  
Author(s):  
Seung Hyun Kim ◽  
◽  
Byung Cho Kim ◽  
◽  
Keyword(s):  
Prior Experience ◽  
Differential Effects ◽  
Resolution Process

Scalable Synthesis of Functionalized Ferrocenyl Azides and Amines Enabled by Flow Chemistry

2019 ◽  
Author(s):  
Merlin Kleoff ◽  
Johannes Schwan ◽  
Lisa Boeser ◽  
Bence Hartmayer ◽  
Mathias Christmann ◽  
...  
Keyword(s):  
Reaction Time ◽  
Heterogeneous Reaction ◽  
Reduction Process ◽  
Flow Chemistry ◽  
Subsequent Reaction ◽  
Scalable Synthesis ◽  
High Yields ◽  
Reactor Section

A scalable access to functionalized 1,1’- and 1,2-ferrocenyl azides has been realized in flow. By halogen‒lithium exchange of ferrocenyl halides and subsequent reaction with tosyl azide, a variety of functionalized ferrocenyl azides was obtained in high yields. To allow a scalable preparation of these potentially explosive compounds, an efficient flow protocol was developed accelerating the reaction time to minutes and circumventing accumulation of potentially hazardous intermediates. Switching from homogeneous to triphasic flow amidst process was key for handling a heterogeneous reaction mixture formed after a heated reactor section. The corresponding and synthetically versatile ferrocenyl amines were then prepared by a reliable reduction process.

Auditors' Communications with Audit Committees: The Influence of the Audit Committee's Oversight Approach

2018 ◽  
Vol 38 (2) ◽  
pp. 125-150 ◽  
Author(s):  
Krista Fiolleau ◽  
Kris Hoang ◽  
Bradley Pomeroy
Keyword(s):  
Audit Committee ◽  
Level Of Detail ◽  
Data Availability ◽  
Audit Committees ◽  
Communication Style ◽  
Quality Audit ◽  
Resolution Process ◽  
Asking Questions

SUMMARY Policymakers have identified effective communications between the auditor and the audit committee (AC) as an indicator of a quality audit, but little is known about the factors auditors consider when deciding what to communicate about significant accounting issues. We propose auditors use the AC's oversight approach as a cue for the level of detail in their communications that is necessary to satisfy the AC's preferences for auditors' insights on issues that were resolved with management. In our experiment, auditors resolved an inventory obsolescence issue with a hypothetical CFO, and then wrote a communication about it for the AC. We manipulate the AC's preference for getting involved in the issue resolution process and its reputation for asking questions. Our results, supplemented by findings from audit partner interviews, suggest auditors tailor their communications to the AC's oversight approach, the AC's industry and accounting knowledge, and the AC chair's preferred communication style. Data Availability: Contact the authors.

Simple and scalable synthesis of urchin-like ZnO nanoparticles via a microwave-assisted drying process

2021 ◽  
Author(s):  
Myung Sik Choi ◽  
Han Gil Na ◽  
Gyu Sam Shim ◽  
Jae Hee Cho ◽  
Min Young Kim ◽  
...  
Keyword(s):  
Zno Nanoparticles ◽  
Drying Process ◽  
Microwave Assisted ◽  
Scalable Synthesis

scholarly journals Towards a Greener and Scalable Synthesis of Na 2 Ti 6 O 13 Nanorods and Their Application as Anodes in Batteries for Grid‐Level Energy Storage

2021 ◽  
Vol 9 (1) ◽  
pp. 2170011
Author(s):  
Dario M. De Carolis ◽  
Dragoljub Vrankovic ◽  
Samira A. Kiefer ◽  
Enrico Bruder ◽  
Michael Thomas Dürrschnabel ◽  
...  
Keyword(s):  
Energy Storage ◽  
Level Energy ◽  
Scalable Synthesis ◽  
Grid Level
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