Synthesis and characterization of zerovalent polynuclear metal carbonyl compounds of chromium, molybdenum, and tungsten. X-ray crystal structure of [Me4N]3[W3(CO)9(.mu.-OC2H5)(.mu.3-OC2H5)2]

1982 ◽  
Vol 1 (5) ◽  
pp. 682-689 ◽  
Author(s):  
John E. Ellis ◽  
Gary L. Rochfort
Keyword(s):  
Crystal Structure ◽  
Carbonyl Compounds ◽  
Metal Carbonyl ◽  
Synthesis And Characterization ◽  
X Ray ◽  
And Tungsten

Darstellung und Charakterisierung von Rubidiumhydrogencyanamid/Synthesis and Characterization of Rubidium Hydrogen Cyanamide

1999 ◽  
Vol 54 (11) ◽  
pp. 1375-1378 ◽  
Author(s):  
Michael Becker ◽  
Martin Jansen
Keyword(s):  
Crystal Structure ◽  
Liquid Ammonia ◽  
Synthesis And Characterization ◽  
Hydrogen Cyanamide ◽  
X Ray ◽  
Bond Lengths

The synthesis of RbHCN2 was carried out by reaction of cyanamide with rubidium amide in liquid ammonia. The crystal structure has been determinedo by x-ray powder methods (orthorhombic, P21,21,21, a = 7.299(1), b = 9.435(1), c = 9.420(1) Å; Z = 8). The anion is slightly bent (174°) and exhibits two different bond lengths (C-N: 1.17, HN-C: 1.31 Å).

The synthesis and characterization of a cationic technetium(V) phenylimido complex. The X-ray crystal structure of [TcCl2(NPh)(PMe2Ph)3](BPh4)

1995 ◽  
Vol 230 (1-2) ◽  
pp. 205-208 ◽  
Author(s):  
Terrence Nicholson ◽  
Alan Davison ◽  
Jon A. Zubieta ◽  
Qin Chen ◽  
Alun G. Jones
Keyword(s):  
Crystal Structure ◽  
Synthesis And Characterization ◽  
X Ray

Synthesis and Characterization of a New Copper(II) Complex with Nadolol, an Aminoalcoholic Beta-blocker. Crystal Structure of Na[Cu(nadololate)(CO3)] · H2O

2008 ◽  
Vol 63 (5) ◽  
pp. 543-547 ◽  
Author(s):  
Inés Viera ◽  
Laura Domínguez ◽  
Javier Ellena ◽  
María H. Torre
Keyword(s):  
Crystal Structure ◽  
Vibrational Spectroscopy ◽  
Copper Complex ◽  
Beta Blocker ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Spectroscopy Analysis ◽  
X Ray

This work reports the synthesis and characterization of a new copper complex with nadolol, a betablocker aminoalcohol. The stoichiometry found was Na[Cu(nadololate)(CO3)] · H2O. Electronic and vibrational spectroscopy analysis was performed, and the crystal structure of Na[Cu(nadololate)-(CO3)] · H2O was determined by X-ray diffraction.

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