scholarly journals Synthesis and characterization of (.eta.5-C5Me5)2Ti(R)Cl (R = Me, Et, n-Pr, CH:CH2, Ph, O-n-Pr) and their salt metathesis reactions. Thermal decomposition pathways of (.eta.5-C5Me5)2Ti(Me)R' (R' = Et, CH:CH2, Ph, CH2Ph)

1992 ◽  
Vol 11 (5) ◽  
pp. 1793-1801 ◽  
Author(s):  
Gerrit A. Luinstra ◽  
Jan H. Teuben
Keyword(s):  
Thermal Decomposition ◽  
Synthesis And Characterization ◽  
Metathesis Reactions

Synthesis and Characterization of Nanocrystalline ZnO Powders by a Direct Thermal Decomposition Route Using Zinc Nitrate Hexahydrate

2013 ◽  
Vol 770 ◽  
pp. 68-71 ◽  
Author(s):  
Supphadate Sujinnapram ◽  
Uraiphorn Termsuk ◽  
Atcharawan Charoentam ◽  
Sutthipoj Sutthana
Keyword(s):  
Thermal Decomposition ◽  
Crystallization Temperature ◽  
Zinc Nitrate ◽  
Zinc Nitrate Hexahydrate ◽  
Absorption Peak ◽  
Synthesis And Characterization ◽  
Nitrate Hexahydrate ◽  
Different Temperatures ◽  
Zno Powders

The nanocrystalline ZnO powders were synthesized by a direct thermal decomposition using zinc nitrate hexahydrate as starting materials. The precursor was characterized by TG-DTA to determine the thermal decomposition and crystallization temperature which was found to be at 325 oC. The precursors were calcined at different temperatures of 400, 500, and 600°C for 4 h. The structure of the prepared samples was studied by XRD, confirming the formation of wurtzite structure. The synthesized powders exhibited the UV absorption below 400 nm (3.10 eV) with a well defined absorption peak at around 285 nm (4.35 eV). The estimated direct bandgaps were obtained to be 3.19, 3.16, and 3.14 eV for the ZnO samples thermally decomposed at 400, 500, and 600°C, respectively.

scholarly journals Synthesis and characterization of ZnO nanoparticles by thermal decomposition of a curcumin zinc complex

2014 ◽  
Vol 7 (6) ◽  
pp. 1178-1184 ◽  
Author(s):  
Mutasim I. Khalil ◽  
Maha M. Al-Qunaibit ◽  
Aisha M. Al-zahem ◽  
Joselito P. Labis
Keyword(s):  
Thermal Decomposition ◽  
Zno Nanoparticles ◽  
Zinc Complex ◽  
Synthesis And Characterization

Synthesis and characterization of NiO nanoclusters via thermal decomposition

Polyhedron ◽  
2009 ◽  
Vol 28 (6) ◽  
pp. 1111-1114 ◽  
Author(s):  
Masoud Salavati-Niasari ◽  
Noshin Mir ◽  
Fatemeh Davar
Keyword(s):  
Thermal Decomposition ◽  
Synthesis And Characterization

scholarly journals Direct synthesis and characterization of mixed-valent Li0.5−δCoPO4, a Li-deficient derivative of the Cmcm polymorph of LiCoPO4

RSC Advances ◽  
2017 ◽  
Vol 7 (45) ◽  
pp. 28069-28081 ◽  
Author(s):  
Jennifer Ludwig ◽  
Carlos Alarcón-Suesca ◽  
Stephan Geprägs ◽  
Dennis Nordlund ◽  
Marca M. Doeff ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Direct Synthesis ◽  
Decomposition Mechanism ◽  
Synthesis And Characterization ◽  
Thermal Decomposition Mechanism

Li0.5−δCoPO4, the first Li-deficient, mixed-valent Co(ii,iii) derivative of Cmcm-LiCoPO4, exhibits a complex, multi-step thermal decomposition mechanism.

Synthesis and Characterization of Co Nanoparticles by Solventless Thermal Decomposition

2007 ◽  
Vol 119 ◽  
pp. 71-74 ◽  
Author(s):  
Yan Li ◽  
Xiao Li Zhang ◽  
Young Hwan Kim ◽  
Young Soo Kang
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Synthesis And Characterization ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Structure Of Nanoparticles ◽  
Co Nanoparticles

Co nanoparticles were synthesized via a solventless thermal decomposition of Co2+-oleate2. The crystalline structure is strongly affected by the thermal treatment of the Co nanoparticles. Further, the annealing also results in the decomposition of surfactant around Co particles. The size of nanoparticles was confirmed by transmission electron microscopy (TEM). The crystal structure of nanoparticles was characterized by X-ray diffraction pattern (XRD). The magnetic properties were characterized by vibrating sample magnetometer (VSM).

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