Supramolecular organolead(IV) and -tin(IV) systems [(Me3EIV)3MIII(CN)6].infin. (E = Pb or Sn, M = Co or Fe): comparative x-ray diffraction and solid-state multinuclear magnetic resonance studies

1992 ◽  
Vol 11 (4) ◽  
pp. 1718-1726 ◽  
Author(s):  
Ulrich Behrens ◽  
Abdul K. Brimah ◽  
Tarek M. Soliman ◽  
R. Dieter Fischer ◽  
David C. Apperley ◽  
...  
Keyword(s):  
Solid State ◽  
Magnetic Resonance ◽  
X Ray Diffraction ◽  
Magnetic Resonance Studies ◽  
X Ray ◽  
Multinuclear Magnetic Resonance

Solid-state and solution 117Sn NMR study of C2O4(SnPh3)2: a revision

2011 ◽  
Vol 34 (5-6) ◽  
pp. 153-153
Author(s):  
Libasse Diop
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Solid State ◽  
Magnetic Resonance ◽  
State Structure ◽  
X Ray Diffraction ◽  
Magnetic Resonance Studies ◽  
X Ray ◽  
Nmr Study ◽  
Tetrahedral Environment ◽  
Good Agreement

Abstract Solid-state and solution 117Sn nuclear magnetic resonance studies of C2O4(SnPh3)2 have been carried out and found to be in good agreement with the tetrahedral environment of the tin (IV) atom as found from the solid state structure, previously determined by a single crystal X-ray diffraction analysis.

1,3,2-Diazaphospha-[3]ferrocenophanes. Molecular Structures and Multinuclear Magnetic Resonance Studies

2009 ◽  
Vol 64 (11-12) ◽  
pp. 1401-1412 ◽  
Author(s):  
Bernd Wrackmeyer ◽  
Elena V. Klimkina ◽  
Wolfgang Milius
Keyword(s):  
Molecular Structure ◽  
Solid State ◽  
Structural Analysis ◽  
Magnetic Resonance ◽  
Phosphorus Atom ◽  
Molecular Structures ◽  
Magnetic Resonance Studies ◽  
X Ray ◽  
Nmr Techniques ◽  
Multinuclear Magnetic Resonance

2-Phenoxy-1,3,2-diazaphospha-[3]ferrocenophane and related derivatives (oxide, sulfide, selenide) were prepared, characterized in solution by multinuclear magnetic resonance methods (1D and 2D 1H, 13C, 15N and 31P NMR) and in the solid state by X-ray structural analysis. The conformation of the 2-phenoxy derivative differs from that of the 2-tert-butyl compound. For further comparison, 2-R- 2,3-dihydro-1H-1,3,2-diazaphospha-phenalene derivatives R = 'Bu, PhO were prepared and studied by the same NMR techniques. The molecular structure of a selenide was determined, and together with the NMR evidence, it was concluded that the conformation of these heterocycles is independent of the respective substituent at the phosphorus atom

Structure of nepetalic acid in the solid state and in solution by x-ray diffraction and nuclear magnetic resonance analysis

1981 ◽  
Vol 46 (16) ◽  
pp. 3302-3305 ◽  
Author(s):  
Edmund J. Eisenbraun ◽  
Clinton E. Browne ◽  
Ernest L. Eliel ◽  
David L. Harris ◽  
Asadur Rahman ◽  
...  
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Solid State ◽  
Magnetic Resonance ◽  
Nuclear Magnetic Resonance Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Resonance Analysis ◽  
Nuclear Magnetic
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