Unsaturated Carbene Transition-Metal Indenyl Complexes. 3. Synthesis and Characterization of (Alkynyl)-, (Vinylidene)-, and (Carbene)ruthenium Indenyl Complexes: X-ray Crystal Structure of [Ru(:C:CMe2)(.eta.5-C9H7)(PPh3)2][CF3SO3].cntdot.1/2CCH2Cl2 and EHMO Calculations

1994 ◽  
Vol 13 (10) ◽  
pp. 4045-4057 ◽  
Author(s):  
M. Pilar Gamasa ◽  
Jose Gimeno ◽  
Blanca M. Martin-Vaca ◽  
Javier Borge ◽  
Santiago Garcia-Granda ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Transition Metal ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Indenyl Complexes

X-ray Crystal Structure of the N-(2-hydroxy-1-naphthalidene)phenylglycine Schiff Base. Synthesis and Characterization of its Transition Metal Complexes

2006 ◽  
Vol 31 (5) ◽  
pp. 580-585 ◽  
Author(s):  
Kalagouda B. Gudasi ◽  
Manjula S. Patil ◽  
Ramesh S. Vadavi ◽  
Rashmi V. Shenoy ◽  
Siddappa A. Patil ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Synthesis And Characterization ◽  
X Ray

Darstellung und Charakterisierung von Rubidiumhydrogencyanamid/Synthesis and Characterization of Rubidium Hydrogen Cyanamide

1999 ◽  
Vol 54 (11) ◽  
pp. 1375-1378 ◽  
Author(s):  
Michael Becker ◽  
Martin Jansen
Keyword(s):  
Crystal Structure ◽  
Liquid Ammonia ◽  
Synthesis And Characterization ◽  
Hydrogen Cyanamide ◽  
X Ray ◽  
Bond Lengths

The synthesis of RbHCN2 was carried out by reaction of cyanamide with rubidium amide in liquid ammonia. The crystal structure has been determinedo by x-ray powder methods (orthorhombic, P21,21,21, a = 7.299(1), b = 9.435(1), c = 9.420(1) Å; Z = 8). The anion is slightly bent (174°) and exhibits two different bond lengths (C-N: 1.17, HN-C: 1.31 Å).

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