Alternative One-Pot Synthesis of (Trifluoromethyl)phenyldiazirines from Tosyloxime Derivatives: Application for New Synthesis of Optically Pure Diazirinylphenylalanines for Photoaffinity Labeling

2015 ◽  
Vol 17 (3) ◽  
pp. 616-619 ◽  
Author(s):  
Lei Wang ◽  
Yuta Murai ◽  
Takuma Yoshida ◽  
Akiko Ishida ◽  
Katsuyoshi Masuda ◽  
...  
Keyword(s):  
Photoaffinity Labeling ◽  
One Pot ◽  
One Pot Synthesis ◽  
New Synthesis ◽  
Optically Pure

A new one-pot synthesis of μ-oxo dimeric iron(III) porphyrins from meso-tetraarylporphyrins

2009 ◽  
Vol 13 (08n09) ◽  
pp. 854-858 ◽  
Author(s):  
Qiang Liu ◽  
Yan-Zhi Gong ◽  
Chang-Jun Gong ◽  
Qing-Hong Li ◽  
Can-Cheng Guo
Keyword(s):  
Synthetic Methods ◽  
High Yield ◽  
Reaction Intermediates ◽  
Ferrous Chloride ◽  
Iron Porphyrins ◽  
One Pot ◽  
Convenient Procedure ◽  
One Pot Synthesis ◽  
New Synthesis ◽  
The One

A new synthesis of μ-oxo dimeric iron(III) porphyrins from meso-tetraarylporphyrins in one-pot procedure is reported. μ-oxo dimeric iron(III) porphyrin was obtained in high yield (up to 93%) from the reaction of meso-tetraarylporphyrin with ferrous chloride in DMF at pH 8–11. Compared with other synthetic methods of μ-oxo dimeric iron(III) porphyrin from meso-tetraarylporphyrins, the one-pot procedure has higher yields of μ-oxo dimeric iron(III) porphyrins and is a simpler and more convenient procedure. In order to evaluate the range of applicability of this method, μ-oxo dimeric iron(III) porphyrins with different substituents were prepared by the reaction of the corresponding meso-tetraarylporphyrins with ferrous chloride. The results showed that it was possible to apply this one-pot procedure to the synthesis of other μ-oxo dimeric iron porphyrins in excellent yields. A mechanism for the formation of μ-oxo dimeric iron porphyrins was proposed based on the reaction intermediates characterized by HPLC and UV-vis methods.

scholarly journals Base-Mediated One-Pot Synthesis of Aliphatic Diazirines for Photoaffinity Labeling

Molecules ◽  
2017 ◽  
Vol 22 (8) ◽  
pp. 1389 ◽  
Author(s):  
Lei Wang ◽  
Zetryana Puteri Tachrim ◽  
Natsumi Kurokawa ◽  
Fumina Ohashi ◽  
Yasuko Sakihama ◽  
...  
Keyword(s):  
Photoaffinity Labeling ◽  
One Pot ◽  
One Pot Synthesis

One-Pot Synthesis of 5,6-Dihydro-8H-dibenzo[a,g]quinolizine-8-ones and Related Isoquinolines; A New Synthesis of Xylopinine

Synthesis ◽  
1980 ◽  
Vol 1980 (10) ◽  
pp. 845-847 ◽  
Author(s):  
Marietta A. Haimova ◽  
Vassil I. Ognyanov ◽  
Nicola M. Mollov
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
New Synthesis

Combining galvanic displacement and in situ polymerization in a new synthesis: micro-composite materials for Li-based batteries

2016 ◽  
Vol 4 (48) ◽  
pp. 18868-18877 ◽  
Author(s):  
P. Sánchez-Fontecoba ◽  
J. M. López del Amo ◽  
N. Fernández ◽  
S. Pérez-Villar ◽  
T. Rojo ◽  
...  
Keyword(s):  
Composite Materials ◽  
In Situ Polymerization ◽  
Galvanic Displacement ◽  
One Pot ◽  
One Pot Synthesis ◽  
New Synthesis ◽  
Displacement Reactions

A novel one-pot synthesis combines galvanic displacement reactions within situpolymerization to obtain organic–inorganic micro-composite materials.

One-pot synthesis of optically pure β-hydroxy sulfones via a heterogeneous ruthenium/diamine-promoted nucleophilic substitution-asymmetric transfer hydrogenation tandem process

2017 ◽  
Vol 7 (19) ◽  
pp. 4444-4450 ◽  
Author(s):  
Jinyu Wang ◽  
Liang Wu ◽  
Xiaoying Hu ◽  
Rui Liu ◽  
Ronghua Jin ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Nucleophilic Substitution ◽  
Transfer Hydrogenation ◽  
Asymmetric Transfer Hydrogenation ◽  
One Pot ◽  
One Pot Synthesis ◽  
Functionalized Mesoporous Silica ◽  
Tandem Process ◽  
The One ◽  
Optically Pure

Chiral ruthenium/diamine-functionalized mesoporous silica is synthesized and its application in the one-pot synthesis of chiral β-hydroxy sulfones is investigated.

ChemInform Abstract: One-Pot Synthesis of Optically Pure Tricyclo(5.3.1.03,8)undecanes Involving a Novel Triple Michael-Dieckmann Reaction.

ChemInform ◽  
2010 ◽  
Vol 28 (7) ◽  
pp. no-no
Author(s):  
S. MAITI ◽  
S. BHADURI ◽  
B. ACHARI ◽  
A. K. BANERJEE ◽  
N. P. NAYAK ◽  
...  
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
Optically Pure

Anionic-Anionic Asymmetric Tandem Reactions: One-Pot Synthesis of Optically Pure Fluorinated Indolines from 2-p-Tolylsulfinyl Alkylbenzenes

2008 ◽  
Vol 47 (41) ◽  
pp. 7941-7944 ◽  
Author(s):  
José Luis García Ruano ◽  
José Alemán ◽  
Silvia Catalán ◽  
Vanesa Marcos ◽  
Silvia Monteagudo ◽  
...  
Keyword(s):  
Tandem Reactions ◽  
One Pot ◽  
One Pot Synthesis ◽  
Optically Pure

One -pot synthesis of optically pure tricyclo[5.3.1.03,8]undecanes involving a novel triple Michael-Dieckmann reaction

1996 ◽  
Vol 37 (44) ◽  
pp. 8061-8062 ◽  
Author(s):  
Soumen Maiti ◽  
Susmita Bhaduri ◽  
Basudeb Achari ◽  
Ashis K. Banerjee ◽  
Nirmalya P. Nayak ◽  
...  
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
Optically Pure
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