Kinetic and Thermodynamic Aspects in the Microwave-Assisted Synthesis of ZnO Nanoparticles in Benzyl Alcohol

ACS Nano ◽  
2009 ◽  
Vol 3 (2) ◽  
pp. 467-477 ◽  
Author(s):  
Idalia Bilecka ◽  
Pierre Elser ◽  
Markus Niederberger
Keyword(s):  
Benzyl Alcohol ◽  
Zno Nanoparticles ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted

Assessment of Magnetic Properties between Fe and Ni Doped ZnO Nanoparticles Synthesized by Microwave Assisted Synthesis Method

2021 ◽  
Vol 317 ◽  
pp. 119-124
Author(s):  
Sabiu Said Abdullahi ◽  
Garba Shehu Musa Galadanci ◽  
Norlaily Mohd Saiden ◽  
Josephine Ying Chyi Liew
Keyword(s):  
Magnetic Properties ◽  
Zno Nanoparticles ◽  
Room Temperature ◽  
Synthesis Method ◽  
Dilute Magnetic Semiconductors ◽  
High Coercivity ◽  
Microwave Assisted Synthesis ◽  
Ferromagnetic Behavior ◽  
Microwave Assisted ◽  
Doped Zno

The emergence of Dilute Magnetic Semiconductors (DMS) with a potentials for spintronic application have attracted much researches attention, special consideration has been given to ZnO semiconductor material due to its wide band gap of 3.37 eV, large exciting binding energy of 60 meV, moreover, its ferromagnetic behavior at room temperature when doped with transition metals. MxZn1-xO (M = Fe or Ni) nanoparticles were synthesized by microwave assisted synthesis method calcined at 600°C. The structural, morphological and magnetic properties of these nanoparticles were studied using X-ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM) and Vibrating Sample Magnetometer (VSM) respectively. Single phase Wurtzite hexagonal crystal structure was observed for the undoped and Fe doped ZnO nanoparticles with no any impurity, whereas Ni doped ZnO nanoparticles shows the formation of NiO impurities. The magnetic measurement reveals a diamagnetic behavior for the undoped ZnO meanwhile a clear room temperature ferromagnetism was observed for both Fe and Ni doped ZnO. Fe doped ZnO present a high saturation magnetization compared to Ni doped ZnO. However, Ni doped ZnO present high coercivity. The research was confirmed that Fe doped ZnO material will be good material combination for spintronic applications.

scholarly journals A facile microwave-assisted synthesis of ZnO nanoparticles and their photocatalytic activity: Effect of pH

2021 ◽  
Vol 18 (2) ◽  
pp. 3-8
Author(s):  
Aura S. Merlano ◽  
Ángel Salazar
Keyword(s):  
Photocatalytic Activity ◽  
Zno Nanoparticles ◽  
Microwave Assisted Synthesis ◽  
Nano Zno ◽  
Effect Of Ph ◽  
Microwave Assisted ◽  
Activity Effect ◽  
Uv Visible

Este estudio reporta una síntesis fácil, libre de surfactantes y asistida por microondas para la producción de nanopartículas de óxido de zinc (ZnO). Se investigó el efecto del valor del pH sobre las propiedades químicas, ópticas, morfológicas y fotocatalíticas de las nanopartículas de ZnO. Las nanopartículas se caracterizaron mediante microscopía electrónica de barrido (SEM), espectroscopía infrarroja por transformada de Fourier (FTIR), espectroscopía de rayos X por dispersión de energía (EDS) y espectroscopía UV-visible (UV-Vis). El análisis SEM muestra que el tamaño de las partículas disminuye con el aumento del valor de pH. Los espectros UV-Vis muestran picos de absorción excitónica alrededor de 334-359 nm. Se encontró que la brecha de energía de las muestras disminuye con el aumento del valor de pH. Finalmente, se evaluó la eficiencia fotocatalítica de los nanomateriales de ZnO mediante la degradación de naranja de metileno (MO) bajo irradiación de luz UV-A y se logró una eficiencia de degradación del colorante del 93.04% para la muestra de ZnO con pH-13. Los resultados experimentales confirman que la ruta propuesta para producir ZnO es fácil, reproducible y amigable con el medio ambiente. Además, el nano ZnO tiene un gran potencial como fotocatalizador para eliminar compuestos orgánicos.

scholarly journals Microwave assisted synthesis of zinc oxide (ZnO) nanoparticles in a noble approach: utilization for antibacterial and photocatalytic activity

2020 ◽  
Vol 2 (5) ◽  
Author(s):  
Kazi Rakib Ahammed ◽  
Md. Ashaduzzaman ◽  
Shujit Chandra Paul ◽  
Mithun Rani Nath ◽  
Snahasish Bhowmik ◽  
...  
Keyword(s):  
Zinc Oxide ◽  
Photocatalytic Activity ◽  
Zno Nanoparticles ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted

Microwave assisted synthesis of ZnO nanoparticles for lighting and dye removal application

2016 ◽  
Vol 480 ◽  
pp. 36-41 ◽  
Author(s):  
Vijay Kumar ◽  
M. Gohain ◽  
S. Som ◽  
Vinod Kumar ◽  
B.C.B. Bezuindenhoudt ◽  
...  
Keyword(s):  
Zno Nanoparticles ◽  
Dye Removal ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted
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