In Situ SHINERS at Electrochemical Single-Crystal Electrode/Electrolyte Interfaces: Tuning Preparation Strategies and Selected Applications

Jian-Feng Li; Alexander Rudnev; Yongchun Fu; Nataraju Bodappa; Thomas Wandlowski

doi:10.1021/nn403444j

In Situ SHINERS at Electrochemical Single-Crystal Electrode/Electrolyte Interfaces: Tuning Preparation Strategies and Selected Applications

ACS Nano ◽

10.1021/nn403444j ◽

2013 ◽

Vol 7 (10) ◽

pp. 8940-8952 ◽

Cited By ~ 38

Author(s):

Jian-Feng Li ◽

Alexander Rudnev ◽

Yongchun Fu ◽

Nataraju Bodappa ◽

Thomas Wandlowski

Keyword(s):

Single Crystal ◽

Single Crystal Electrode

Download Full-text

Molecular Assembly and Electropolymerization of 3,4-Ethylenedioxythiophene on Au(111) Single Crystal Electrode as Probed by In Situ Electrochemical STM in 0.10 M HClO4

Langmuir ◽

10.1021/la100558x ◽

2010 ◽

Vol 26 (13) ◽

pp. 10771-10777 ◽

Cited By ~ 20

Author(s):

Lorico D. S. Lapitan ◽

Bernard John V. Tongol ◽

Shueh-Lin Yau

Keyword(s):

Single Crystal ◽

Molecular Assembly ◽

Single Crystal Electrode

Download Full-text

In situ scanning tunneling microscopy imaging of electropolymerized poly(3,4-ethylenedioxythiophene) on an iodine-modified Au(111) single crystal electrode

Electrochimica Acta ◽

10.1016/j.electacta.2011.12.053 ◽

2012 ◽

Vol 62 ◽

pp. 433-440 ◽

Cited By ~ 10

Author(s):

Lorico D.S. Lapitan ◽

Bernard John V. Tongol ◽

Shueh-Lin Yau

Keyword(s):

Single Crystal ◽

Scanning Tunneling Microscopy ◽

Scanning Tunneling ◽

Tunneling Microscopy ◽

Microscopy Imaging ◽

Single Crystal Electrode

Download Full-text

An in-situ X-ray diffraction study on the electrochemical formation of PtZn alloys on Pt(1 1 1) single crystal electrode

Applied Surface Science ◽

10.1016/j.apsusc.2015.04.072 ◽

2015 ◽

Vol 354 ◽

pp. 443-449 ◽

Cited By ~ 3

Author(s):

J. Drnec ◽

D. Bizzotto ◽

F. Carlà ◽

R. Fiala ◽

A. Sode ◽

...

Keyword(s):

Single Crystal ◽

Diffraction Study ◽

X Ray Diffraction ◽

X Ray ◽

Single Crystal Electrode

Download Full-text

In situ real-time study on potential induced structure change at Au(111) and Au(100) single crystal electrode/sulfuric acid solution interfaces by surface x-ray scattering

Surface Science ◽

10.1016/j.susc.2014.06.013 ◽

2015 ◽

Vol 631 ◽

pp. 96-104 ◽

Cited By ~ 13

Author(s):

Toshihiro Kondo ◽

Jörg Zegenhagen ◽

Satoru Takakusagi ◽

Kohei Uosaki

Keyword(s):

Sulfuric Acid ◽

Acid Solution ◽

Single Crystal ◽

Structure Change ◽

Time Study ◽

X Ray ◽

X Ray Scattering ◽

Single Crystal Electrode ◽

Induced Structure

Download Full-text

Dynamic self-assembly and electropolymerization processes of 3,4-ethylenedioxythiophene on Au(100) single crystal electrode as probed by in situ scanning tunneling microscopy

Electrochimica Acta ◽

10.1016/j.electacta.2012.04.010 ◽

2012 ◽

Vol 71 ◽

pp. 302-309 ◽

Cited By ~ 5

Author(s):

Jonyl L. Garcia ◽

Bernard John V. Tongol ◽

Shueh-Lin Yau

Keyword(s):

Single Crystal ◽

Scanning Tunneling Microscopy ◽

Self Assembly ◽

Scanning Tunneling ◽

Tunneling Microscopy ◽

Single Crystal Electrode

Download Full-text

In situ scanning tunneling microscopy studies of thiocyanate adlayers on Pt(111) single crystal electrode surfaces

Electrochimica Acta ◽

10.1016/s0013-4686(97)10183-9 ◽

1998 ◽

Vol 43 (18) ◽

pp. 2619-2626 ◽

Cited By ~ 3

Author(s):

Qiyuan Peng ◽

J.J. Breen

Keyword(s):

Single Crystal ◽

Scanning Tunneling Microscopy ◽

Scanning Tunneling ◽

Tunneling Microscopy ◽

Electrode Surfaces ◽

Single Crystal Electrode

Download Full-text

Second harmonic generation study of the reconstruction of an Au(110) electrode in HClO4

Canadian Journal of Chemistry ◽

10.1139/v97-051 ◽

1997 ◽

Vol 75 (4) ◽

pp. 449-455 ◽

Cited By ~ 5

Author(s):

C. Dale Keefe ◽

Erika Revesz ◽

Michel Dionne ◽

Mario Morin

Keyword(s):

Second Harmonic Generation ◽

Single Crystal ◽

Harmonic Generation ◽

Second Harmonic ◽

Large Component ◽

In Situ Study ◽

Threefold Symmetry ◽

Single Crystal Electrode ◽

Second Harmonic Generation Spectroscopy

Second harmonic generation (SHG) was used to carry out an in situ study of the potential-induced reconstruction of an Au(110) single crystal electrode in an aqueous solution of 0.01 M HClO4. In this study, we found that the symmetries of the surface susceptibility of the reconstructed and the unreconstructed Au(110) surfaces have a large component of threefold symmetry. A detailed analysis shows that both surfaces have an overall Cs symmetry giving one-, two-, and threefold symmetries for the surface susceptibility. However, another, different, source of threefold symmetry, perpendicular to the first, is needed to fit the data. We suggest that this extra source of threefold symmetry is due to the (111) microfacets that are present on the open (110) surface. Keywords: electrochemistry, single crystal, reconstruction, second harmonic generation spectroscopy.

Download Full-text