Lamellar Thickening Growth of an Extended Chain Single Crystal of Polyethylene. 1. Pointers to a New Crystallization Mechanism of Polymers

1997 ◽  
Vol 30 (7) ◽  
pp. 2067-2074 ◽  
Author(s):  
M. Hikosaka ◽  
K. Amano ◽  
S. Rastogi ◽  
A. Keller
Keyword(s):  
Single Crystal ◽  
Crystallization Mechanism ◽  
Extended Chain

Lamellar Thickening Growth of an Isolated Extended Chain Single Crystal of PE

1993 ◽  
pp. 331-336 ◽  
Author(s):  
M. Hikosaka ◽  
K. Amano ◽  
S. Rastogi ◽  
A. Keller
Keyword(s):  
Single Crystal ◽  
Extended Chain

Reaction of oxygen with a binuclear cobalt(II) hexaphosphine complex. Single-crystal X-ray structure of an extended chain cobalt(II) hexaphosphine oxide system

Polyhedron ◽  
1988 ◽  
Vol 7 (18) ◽  
pp. 1785-1788 ◽  
Author(s):  
Suzanne E. Saum ◽  
Fredric R. Askham ◽  
Frank R. Fronczek ◽  
George G. Stanley
Keyword(s):  
Single Crystal ◽  
Oxide System ◽  
X Ray ◽  
Extended Chain

scholarly journals Molecular Weight Dependence of Primary Nucleation Rate of Polyethylene I. An Extended Chain Single Crystal

1999 ◽  
Vol 31 (9) ◽  
pp. 749-758 ◽  
Author(s):  
Mutsuo Nishi ◽  
Masamichi Hikosaka ◽  
Swapan Kumer Ghosh ◽  
Akihiko Toda ◽  
Koji Yamada
Keyword(s):  
Molecular Weight ◽  
Single Crystal ◽  
Nucleation Rate ◽  
Primary Nucleation ◽  
Molecular Weight Dependence ◽  
Extended Chain

Molecular weight dependence of lateral growth rate of polyethylene (I) — an extended chain single crystal

Polymer ◽  
1998 ◽  
Vol 39 (8-9) ◽  
pp. 1591-1596 ◽  
Author(s):  
Mutsuo Nishi ◽  
Masamichi Hikosaka ◽  
Akihiko Toda ◽  
Masato Takahashi
Keyword(s):  
Molecular Weight ◽  
Growth Rate ◽  
Single Crystal ◽  
Lateral Growth ◽  
Molecular Weight Dependence ◽  
Extended Chain ◽  
Lateral Growth Rate

A Preparation of High Resolution Standards for Electron Microscopy. Part II

1971 ◽  
Vol 29 ◽  
pp. 160-161
Author(s):  
Akira Tanaka ◽  
David F. Harling
Keyword(s):  
Electron Microscopy ◽  
High Resolution ◽  
Carbon Black ◽  
Single Crystal ◽  
Dark Field ◽  
Graphitized Carbon Black ◽  
Graphitized Carbon ◽  
Dark Field Imaging ◽  
Crystal Films ◽  
Micro Holes

In the previous paper, the author reported on a technique for preparing vapor-deposited single crystal films as high resolution standards for electron microscopy. The present paper is intended to describe the preparation of several high resolution standards for dark field microscopy and also to mention some results obtained from these studies. Three preparations were used initially: 1.) Graphitized carbon black, 2.) Epitaxially grown particles of different metals prepared by vapor deposition, and 3.) Particles grown epitaxially on the edge of micro-holes formed in a gold single crystal film.The authors successfully obtained dark field micrographs demonstrating the 3.4Å lattice spacing of graphitized carbon black and the Au single crystal (111) lattice of 2.35Å. The latter spacing is especially suitable for dark field imaging because of its preparation, as in 3.), above. After the deposited film of Au (001) orientation is prepared at 400°C the substrate temperature is raised, resulting in the formation of many square micro-holes caused by partial evaporation of the Au film.

Structure of Palladium Single-Crystal Films Prepared by Flash Evaporation onto (001) NaCl Substrates

1970 ◽  
Vol 28 ◽  
pp. 456-457
Author(s):  
L. E. Murr ◽  
G. Wong
Keyword(s):  
Single Crystal ◽  
High Vacuum ◽  
Ultra High Vacuum ◽  
High Rate ◽  
Flash Evaporation ◽  
Optimum Load ◽  
Single Crystal Films ◽  
Crystal Films ◽  
A Current

Palladium single-crystal films have been prepared by Matthews in ultra-high vacuum by evaporation onto (001) NaCl substrates cleaved in-situ, and maintained at ∼ 350° C. Murr has also produced large-grained and single-crystal Pd films by high-rate evaporation onto (001) NaCl air-cleaved substrates at 350°C. In the present work, very large (∼ 3cm2), continuous single-crystal films of Pd have been prepared by flash evaporation onto air-cleaved (001) NaCl substrates at temperatures at or below 250°C. Evaporation rates estimated to be ≧ 2000 Å/sec, were obtained by effectively short-circuiting 1 mil tungsten evaporation boats in a self-regulating system which maintained an optimum load current of approximately 90 amperes; corresponding to a current density through the boat of ∼ 4 × 104 amperes/cm2.

Dislocations, Ordering and Antiferromagnetic Domains in MnO

1970 ◽  
Vol 28 ◽  
pp. 522-523
Author(s):  
D. J. Barber ◽  
R. G. Evans
Keyword(s):  
Electron Diffraction ◽  
Single Crystal ◽  
Optical Microscopy ◽  
Defect Chemistry ◽  
Magnetic Structures ◽  
Optically Transparent ◽  
Magnetic Features ◽  
Antiferromagnetic Domains

Manganese (II) oxide, MnO, in common with CoO, NiO and FeO, possesses the NaCl structure and shows antiferromagnetism below its Neel point, Tn∼ 122 K. However, the defect chemistry of the four oxides is different and the magnetic structures are not identical. The non-stoichiometry in MnO2 small (∼2%) and below the Tn the spins lie in (111) planes. Previous work reported observations of magnetic features in CoO and NiO. The aim of our work was to find explanations for certain resonance results on antiferromagnetic MnO.Foils of single crystal MnO were prepared from shaped discs by dissolution in a mixture of HCl and HNO3. Optical microscopy revealed that the etch-pitted foils contained cruciform-shaped precipitates, often thick and proud of the surface but red-colored when optically transparent (MnO is green). Electron diffraction and probe microanalysis indicated that the precipitates were Mn2O3, in contrast with recent findings of Co3O4 in CoO.

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