Morphological Studies of Oriented Crystallization of High-Density Polyethylene

1978 ◽  
Vol 11 (6) ◽  
pp. 1210-1215 ◽  
Author(s):  
Takeji Hashimoto ◽  
Satoshi Ishido ◽  
Hiromichi Kawai ◽  
Andrzej Ziabicki
Keyword(s):  
High Density Polyethylene ◽  
High Density ◽  
Morphological Studies ◽  
Oriented Crystallization

scholarly journals Effects of heat energy on morphology and properties of selective inhibition sintered high density polyethylene

2019 ◽  
Vol 13 (1) ◽  
pp. 4403-4414 ◽  
Author(s):  
Rajamani D ◽  
E Balasubramanian
Keyword(s):  
High Density Polyethylene ◽  
Structural Integrity ◽  
Threshold Level ◽  
Selective Inhibition ◽  
Heat Energy ◽  
High Density ◽  
Selective Inhibition Sintering ◽  
Morphological Studies ◽  
Property Evaluation ◽  
The Impact

This study provides an account of comprehensive experimentation and mechanical characterisation of high density polyethylene (HDPE) parts that are fabricated through an additive manufacturing process called selective inhibition sintering (SIS). In this study, test specimens are fabricated by selective fusing of HDPE particles through controlled heating. Morphological studies and mechanical property evaluation of these specimens are carried out to assess the impact of energy on sintering of HDPE particles and structural integrity. Results indicate that, heat energy up to a threshold level of 28.48 J/mm2 results in superior fusion of the HDPE particles, and further increase causes degradation of the structure. Surface roughness, tensile and flexural properties of SIS parts are compared with those of injection moulded parts for assessing their suitability to engineering applications.

Composition and Surface Topography Effects on Apatite-Forming Ability of Ceramic-Polymer Composites

2003 ◽  
Vol 774 ◽  
Author(s):  
Susan M. Rea ◽  
Serena M. Best ◽  
William Bonfield
Keyword(s):  
Surface Topography ◽  
High Density Polyethylene ◽  
High Density ◽  
Apatite Layer ◽  
Biologically Active ◽  
Human Blood Plasma ◽  
Apatite Formation ◽  
Polyethylene Matrix ◽  
Composite Surface ◽  
X Ray

AbstractHAPEXTM (40 vol% hydroxyapatite in a high-density polyethylene matrix) and AWPEX (40 vol% apatite-wollastonite glass ceramic in a high density polyethylene matrix) are composites designed to provide bioactivity and to match the mechanical properties of human cortical bone. HAPEXTM has had clinical success in middle ear and orbital implants, and there is great potential for further orthopaedic applications of these materials. However, more detailed in vitro investigations must be performed to better understand the biological interactions of the composites and so the bioactivity of each material was assessed in this study. Specifically, the effects of controlled surface topography and ceramic filler composition on apatite layer formation in acellular simulated body fluid (SBF) with ion concentration similar to those of human blood plasma were examined. Samples were prepared as 1 cm × 1 cm × 1 mm tiles with polished, roughened, or parallel-grooved surface finishes, and were incubated in 20 ml of SBF at 36.5 °C for 1, 3, 7, or 14 days. The formation of a biologically active apatite layer on the composite surface after immersion was demonstrated by thin-film x-ray diffraction (TF-XRD), environmental scanning electron microscopy (ESEM) imaging and energy dispersive x-ray (EDX) analysis. Variations in sample weight and solution pH over the period of incubation were also recorded. Significant differences were found between the two materials tested, with greater bioactivity in AWPEX than HAPEXTM overall. Results also indicate that within each material the surface topography is highly important, with rougher samples correlated to earlier apatite formation.

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