Molecular Mobility of Amorphous Chain Segments of Ethylene−Methyl Methacrylate Copolymer Films as a Function of Temperature Estimated by Positron Annihilation, X-ray Diffraction, and13C NMR

2003 ◽  
Vol 36 (21) ◽  
pp. 8056-8065 ◽  
Author(s):  
Lin Ma ◽  
Chunqing He ◽  
Takenori Suzuki ◽  
Mami Azuma ◽  
Yuezhen Bin ◽  
...  
1995 ◽  
Vol 78 (3) ◽  
pp. 1510-1513 ◽  
Author(s):  
S. Fujii ◽  
Y. Nishibayashi ◽  
S. Shikata ◽  
A. Uedono ◽  
S. Tanigawa

2009 ◽  
Vol 79-82 ◽  
pp. 353-356
Author(s):  
Wei Pan ◽  
Yan Chen ◽  
Xiao Wei He

The polyacrylonitrile(PAN)/poly (methyl methacrylate)(PMMA) blend fibers were prepared by wet-spinning technique and carbonized over the temperature range of 400-1000°C in nitrogen atmosphere. After carbonization of the blend fibers, the PMMA component removed and the PAN component left in the form of carbon nanofibers. Morphology of the carbon nanofibers were investigated via scanning electron microscopy (SEM), and the carbonization behavior of the fibers were examined via x-ray diffraction (XRD), Raman microspectrometry. The optimal condition made carbon fibers with great L/D ratio and diameter less than 200 nm. XRD and Raman spectra shows that the PAN/PMMA blend fibers treated at 600°C produced some graphite crystallite.


1984 ◽  
Vol 16 (1) ◽  
pp. 15-20 ◽  
Author(s):  
Stephen Doyle ◽  
Bansi D. Malhotra ◽  
Norman Peacock ◽  
Richard A. Pethrick

Author(s):  
Jayashree Bagawade ◽  

A series of novel zinc oxide / Poly (methyl methacrylate) nanocomposite films with different ZnO contents were prepared through inclusion of pre-synthesized zinc oxide nanoparticles. The physical composition and morphology of the as-prepared nanocomposites were studied by XRD and TEM. The TEM analyses revealed that the zinc oxide nanoparticles have a particle size of ~3–5 nm. X-ray diffraction proved the presence of the amorphous PMMA in the nanocomposites. The intermolecular interactions within the polymer nanocomposites were explored by FTIR and XRD. FTIR spectra confirmed the dispersion of the zinc oxide nanoparticles in the Poly (methyl methacrylate) i.e. PMMA matrices. The UV-Vis absorption measurements of the ZnO/PMMA nanocomposites proved their potential optical properties.


2019 ◽  
Vol 6 (8) ◽  
pp. 2167-2177 ◽  
Author(s):  
K. Sudarshan ◽  
V. Tiwari ◽  
P. Utpalla ◽  
S. K. Gupta

Defects and their influence on light emitting properties were explored in CeO2:Eu,Nb using Rietveld refinement, positron annihilation and luminescence spectroscopy.


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