Synthesis and Characterization of Amphiphilic Biomimetic Assemblies at Electrochemically Active Surfaces

Langmuir ◽  
2003 ◽  
Vol 19 (9) ◽  
pp. 3875-3882 ◽  
Author(s):  
Paweł Krysiński ◽  
G. J. Blanchard
Keyword(s):  
Synthesis And Characterization ◽  
Active Surfaces ◽  
Electrochemically Active

Synthesis and characterization of dendritic platinum bisferrocenylacetylide complexes

2012 ◽  
Vol 90 (3) ◽  
pp. 278-289
Author(s):  
Qing Han ◽  
Li-Jun Chen ◽  
Hai-Bo Yang ◽  
Quan-Jie Li ◽  
Jiuming He ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Diffusion Coefficient ◽  
Coupling Reaction ◽  
Synthesis And Characterization ◽  
Electrochemical Studies ◽  
Maldi Tof Ms ◽  
Electrochemically Active ◽  
Key Steps ◽  
Tof Ms

A series of new dendritic platinum bisferrocenylacetylide complexes have been synthesized utilizing the coupling reaction of trans-Pt complexes with C–H bonds in alkynes as key steps. These new bimetallic dendrimers were fully characterized by multinuclear NMR (1H, 13C, and 31P) and mass spectrometry (MALDI-TOF-MS and CSI-TOF-MS). Electrochemical studies of these complexes were carried out and revealed that all of the redox moieties are stable, independent, and electrochemically active. In addition, all metallodendrimers show one-electron reaction responses, and the increased sizes of these complexes did not exhibit a dramatic influence on the diffusion coefficient.

Design, synthesis, and characterization of an Fe(ii)-polymer of a redox non-innocent, heteroatomic, polydentate Schiff's base ligand: negative differential resistance and memory behaviour

2018 ◽  
Vol 42 (23) ◽  
pp. 19090-19100 ◽  
Author(s):  
Deepa Oberoi ◽  
Parveen Dagar ◽  
Uday Shankar ◽  
Giriraj Vyas ◽  
Anil Kumar ◽  
...  
Keyword(s):  
Negative Differential Resistance ◽  
Differential Resistance ◽  
Complete Characterization ◽  
Synthesis And Characterization ◽  
Schiff’S Base ◽  
Design Synthesis ◽  
Electrochemically Active ◽  
Hexadentate Ligand

Complete characterization and memristive study of the electrochemically active, novel Fe(ii)-polymer of a fluorescence active conjugated, hexadentate ligand.

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

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