Structure and Dynamics of Hydrous Surface Species on Alumina−Boria Catalysts and Their Precursors from 1H, 2H, 11B, and 27Al MAS NMR Spectroscopy

2009 ◽  
Vol 113 (6) ◽  
pp. 2475-2486 ◽  
Author(s):  
Michael Ryan Hansen ◽  
Hans J. Jakobsen ◽  
Jørgen Skibsted
2001 ◽  
Vol 203 (2) ◽  
pp. 375-381 ◽  
Author(s):  
Irina I Ivanova ◽  
Elena B Pomakhina ◽  
Alexander I Rebrov ◽  
Michael Hunger ◽  
Yuryi G Kolyagin ◽  
...  

1991 ◽  
Vol 46 (11) ◽  
pp. 1515-1518 ◽  
Author(s):  
Gerhard Wegner ◽  
Gert Blumenthal ◽  
Dirk Müller ◽  
Dirk-Henning Menz ◽  
Antje Schmalstieg

Products of the thermolysis of NH4Al-alum were prepared under dried air and characterized by X-ray powder diffraction, thermogravimetry, and for the first time by solid-state 27Al-MAS-NMR spectroscopy. It was found, that high resolution NMR spectroscopy is applicable to follow up the thermal decomposition and to indicate even minor structural changes. 27Al-MAS-NMR spectra show peaks with characteristic chemical shifts for octahedral Al-units up to a high stage of thermolysis. During the decomposition of Al2(SO4)3 to γ-Al2O3 we again observed three-peak spectra with the specific signal at ≈ 35 ppm for penta-coordinated Al ions as recently proved for the thermolysis of AlCl3 · 6 H2O.


2009 ◽  
Vol 25 (3) ◽  
pp. 290-295 ◽  
Author(s):  
Norhazlin Zainuddin ◽  
Natalia Karpukhina ◽  
Robert G. Hill ◽  
Robert V. Law

1991 ◽  
Vol 26 (18) ◽  
pp. 5053-5059 ◽  
Author(s):  
J. Senegas ◽  
A. R. Grimmer ◽  
D. Muller ◽  
P. Thomas ◽  
D. Mercurio ◽  
...  

1992 ◽  
Vol 25 (10) ◽  
pp. 2746-2751 ◽  
Author(s):  
Parshuram G. Shukla ◽  
Swaminathan Sivaram ◽  
Baijayantimala Mohanty

1996 ◽  
Vol 47 (1) ◽  
pp. 125-130 ◽  
Author(s):  
R. LOOKMAN ◽  
H. GEERTS ◽  
P. GROBET ◽  
R. MERCKX ◽  
K. VLASSAK

2007 ◽  
Vol 328 (2) ◽  
pp. 174-182 ◽  
Author(s):  
Luz Rodríguez-González ◽  
Florian Hermes ◽  
Marko Bertmer ◽  
Enrique Rodríguez-Castellón ◽  
Antonio Jiménez-López ◽  
...  

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