Facile One-Pot Solution Phase Synthesis of SnO2Nanotubes

2008 ◽  
Vol 112 (33) ◽  
pp. 12616-12622 ◽  
Author(s):  
Ning Wang ◽  
Xia Cao ◽  
Lin Guo
Keyword(s):  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

ChemInform Abstract: One-Pot Parallel Solution-Phase Synthesis of 1-Substituted 4-(2-Aminoethyl)-1H-pyrazol-5-ols.

ChemInform ◽  
2009 ◽  
Vol 40 (4) ◽  
Author(s):  
David Kralj ◽  
Ana Novak ◽  
Georg Dahmann ◽  
Uros Groselj ◽  
Anton Meden ◽  
...  
Keyword(s):  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Parallel Solution ◽  
Solution Phase Synthesis

One-pot Solution-phase Synthesis of Paramagnetic Co2P Nanorods

2004 ◽  
Vol 33 (10) ◽  
pp. 1272-1273 ◽  
Author(s):  
Hongwei Hou ◽  
Qing Yang ◽  
Chenrong Tan ◽  
Guangbin Ji ◽  
Benxi Gu ◽  
...  
Keyword(s):  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

One-Pot Synthesis of Multi-Branched FeO(OH) Nanorods

2010 ◽  
Vol 663-665 ◽  
pp. 914-917
Author(s):  
De Hui Sun ◽  
Ji Lin Zhang ◽  
De Xin Sun ◽  
Yu Hao
Keyword(s):  
Synthesis Method ◽  
Alcohol Solution ◽  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
X Ray ◽  
Reaction Solution ◽  
Solution Phase Synthesis ◽  
Morphology And Structure ◽  
Scanning Electron

Multi-branched FeO(OH) nanorods are successfully prepared using a facile one-pot solution-phase synthesis method. Their morphology and structure were characterized using field emission scanning electron microscopy (FE-SEM), X-ray powder diffraction (XRD), and Fourier transform infrared (FTIR) absorption spectrum. The results show amount of surfactant (PEO)20(PPO)70(PEO)20 (P123) and precipitant hexamethylenetetramine (HMTA) have significant effect on the shape of the particles. When 20-25 g of the P123 alcohol solution (20 wt%) is added the reaction solution containing 5.0 mL HMTA (2 mol/L) or when 18 g of the P123 alcohol solution (20 wt%) is added the reaction solution containing 10.0 mL HMTA (2 mol/L), the multi-branched FeO(OH) nanorods can be obtained. While when 19-22 g of the P123 alcohol solution (20 wt%) is added the reaction solution containing 10.0 mL HMTA (2 mol/L), the products became the Fe3O4 nanosheets with irregular shape. A possible growth mechanism of the multi-branched FeO(OH) nanorods is suggested.

One-Pot Solution-Phase Synthesis of Paramagnetic Co2P Nanorods.

ChemInform ◽  
2005 ◽  
Vol 36 (5) ◽  
Author(s):  
Hongwei Hou ◽  
Qing Yang ◽  
Chenrong Tan ◽  
Guangbin Ji ◽  
Benxi Gu ◽  
...  
Keyword(s):  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

One-Pot Parallel Solution-Phase Synthesis of 1-Substituted 4-(2-Aminoethyl)-1H-pyrazol-5-ols†

2008 ◽  
Vol 10 (5) ◽  
pp. 664-670 ◽  
Author(s):  
David Kralj ◽  
Ana Novak ◽  
Georg Dahmann ◽  
Uroš Grošelj ◽  
Anton Meden ◽  
...  
Keyword(s):  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Parallel Solution ◽  
Solution Phase Synthesis

scholarly journals One-pot synthesis of sub-10 nm LiNbO3 nanocrystals exhibiting a tunable optical second harmonic response

2019 ◽  
Vol 1 (6) ◽  
pp. 2268-2275 ◽  
Author(s):  
Rana Faryad Ali ◽  
Matthew Bilton ◽  
Byron D. Gates
Keyword(s):  
Second Harmonic ◽  
Optical Response ◽  
Solution Phase ◽  
One Pot ◽  
Phase Synthesis ◽  
Single Crystalline ◽  
Harmonic Response ◽  
One Pot Synthesis ◽  
Solution Phase Synthesis ◽  
Non Linear

Sub-10 nm single-crystalline LiNbO3, nanocrystals that exhibit a tunable non-linear optical response were prepared by a one-pot solution-phase synthesis.

Enhancing thermoelectric performance through one-pot solution phase synthesis of Bi2S3 nanobundles

2016 ◽  
Vol 185 ◽  
pp. 67-71 ◽  
Author(s):  
Hong Chen ◽  
Ting Huang ◽  
Shuqi Zheng ◽  
Teng Fang ◽  
Lijun Wang
Keyword(s):  
Solution Phase ◽  
Thermoelectric Performance ◽  
One Pot ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

Non-Hydrolytic Solution-Phase Synthesis of Anisotropic LiNbO3 and Nb2O5 Nanostructures

2008 ◽  
Vol 1087 ◽  
Author(s):  
Bryan D. Wood ◽  
Byron D. Gates
Keyword(s):  
Crystal Size ◽  
Triphenylphosphine Oxide ◽  
Solution Phase ◽  
One Pot ◽  
Experimental Procedure ◽  
Phase Synthesis ◽  
Aspect Ratios ◽  
Solution Phase Synthesis ◽  
Size And Morphology ◽  
The Stability

AbstractThis paper describes an innovative and simple technique to synthesize anisotropic nanostructures of both lithium niobate (LiNbO3) and niobium oxide (Nb2O5). These materials were obtained using a solution-phase non-hydrolytic decomposition of LiNb(OPri)6 with or without the presence of Nb and Li-chlorides. The stability of LiCl is suggested as an explanation for the lack of LiNbO3 production in the chloride-based reaction. After 2 and 24 hours of reaction crystalline products of Nb2O5 and LiNbO3 are obtained without further thermal treatment. The products of both reactions contained a mixture of spherical and rod-like morphologies. Larger crystals of LiNbO3 and Nb2O5 were predominantly found to be anisotropic with aspect ratios of 7:1 and 3:1, respectively. These structures are believed to result from the natural anisotropy of the unit cell for these materials and from the use of triphenylphosphine oxide (TPPO) as a coordinating solvent. Our solution-phase synthesis is easily scaled-up as a one-pot procedure that offers a promising route to controlling crystal size and morphology. Details of the composition and the growth of our LiNbO3 and Nb2O5 nanostructures will be discussed in addition to the details of our experimental procedure.

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