NMR Study of BA/FBA Cocrystal Confined Within Mesoporous Silica Nanoparticles Employing Thermal Solid Phase Transformation

2015 ◽  
Vol 119 (16) ◽  
pp. 8652-8661 ◽  
Author(s):  
Ewa Skorupska ◽  
Piotr Paluch ◽  
Agata Jeziorna ◽  
Marek J. Potrzebowski
Keyword(s):  
Phase Transformation ◽  
Mesoporous Silica ◽  
Silica Nanoparticles ◽  
Solid Phase ◽  
Mesoporous Silica Nanoparticles ◽  
Nmr Study ◽  
Solid Phase Transformation

Solid-State NMR Study of MCM-41-type Mesoporous Silica Nanoparticles

2005 ◽  
Vol 127 (9) ◽  
pp. 3057-3068 ◽  
Author(s):  
Julien Trébosc ◽  
Jerzy W. Wiench ◽  
Seong Huh ◽  
Victor S.-Y. Lin ◽  
Marek Pruski
Keyword(s):  
Solid State ◽  
Mesoporous Silica ◽  
Silica Nanoparticles ◽  
Solid State Nmr ◽  
Mesoporous Silica Nanoparticles ◽  
Nmr Study ◽  
Mcm 41

Solid-phase extraction of phospholipids using mesoporous silica nanoparticles: application to human milk samples

2018 ◽  
Vol 410 (20) ◽  
pp. 4847-4854 ◽  
Author(s):  
Héctor Martínez Pérez-Cejuela ◽  
Isabel Ten-Doménech ◽  
Jamal El Haskouri ◽  
Pedro Amorós ◽  
Ernesto F. Simó-Alfonso ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Solid Phase Extraction ◽  
Human Milk ◽  
Silica Nanoparticles ◽  
Solid Phase ◽  
Mesoporous Silica Nanoparticles ◽  
Phase Extraction ◽  
Milk Samples

scholarly journals In vitro speciation of molybdenum in human biological samples based on thiol functionalized mesoporous silica nanoparticles and hexyl-methylimidazolium tris-pentafluoroethyl-trifluorophosphate

2020 ◽  
Vol 3 (03) ◽  
pp. 54-64
Author(s):  
Roya Ashori ◽  
Seyed Alireza Hajiseyed Mirzahosseini
Keyword(s):  
Ionic Liquid ◽  
Mesoporous Silica ◽  
Silica Nanoparticles ◽  
Biological Samples ◽  
Solid Phase ◽  
Mesoporous Silica Nanoparticles ◽  
Electrothermal Atomic Absorption Spectrometry ◽  
Serum Samples ◽  
Functionalized Mesoporous Silica

Molybdenum (Mo) ions enter to human body from the diet or drinking waters and have a potentially toxic effect on humans. The thiol-functionalized mesoporous silica nanoparticles (HS-MSNPs) were used for determination and speciation of Mo (II, VI) in human biological samples by dispersive ionic liquid-micro-solid phase extraction (DIL-μ-SPE) coupled to electrothermal atomic absorption spectrometry (ET-AAS). Firstly, the mixture of HS-MSNPs (15 mg), the hydrophobic ionic liquid (1-Hexyl-3-methylimidazolium tris(pentafluoroethyl) trifluorophosphate; [HMIM][T(PFE)PF3]) and acetone injected into 10 mL of human blood and serum samples. After shaking for 5 min, the Mo(II) and Mo(VI) ions were extracted with the thiol group of MSNPs at pH 6 and 2, respectively, and collected through IL at the bottom of the conical tube by centrifuging. Then, the MO(II,VI) ions were back-extracted from HS-MSNPs with elent based on changing pH, and remained solutions were determined by ET-AAS after dilution with DW up to 0.5 mL, separately.

scholarly journals Air Pollution Method: A new method based on ionic liquid passed on mesoporous silica nanoparticles for removal of manganese dust in the workplace air

2019 ◽  
Vol 2 (01) ◽  
pp. 5-14 ◽  
Author(s):  
Parisa Paydar ◽  
Ali Faghihi Zarandi
Keyword(s):  
Ionic Liquid ◽  
Mesoporous Silica ◽  
Silica Nanoparticles ◽  
Solid Phase ◽  
Mesoporous Silica Nanoparticles ◽  
Adsorption Method ◽  
Adsorption Removal ◽  
Workplace Air ◽  
Set Up ◽  
System 1

Chronic effect of manganese exposure to humans caused the dysfunction of nervous system. An applied sorbent based on hydrophobic ionic liquid passed on mesoporous silica nanoparticles was used for adsorption/removal of manganese dust (Mn) from workplace air by solid phase adsorption method. In bench scale set up, 5 mL of standard solution of nitrate and oxide of Mn (0.2-5 mg L-1) was used for generation of manganese dust in pure air by drying procedure, and then was passed through column of IL/MSNPs by SKC pump with flow rate  of 200-500 mL min-1 by SKC pump. The Mn particles separated from column of IL/MSNPs by irrigation of nitric acid solution before determined by F-AAS/ET-AAS. In optimized conditions, the adsorption capacity of MSNPs and IL/MSNPs for Mn removal from air in batch system (1 Li) was obtained 118.5 mg g-1 and 216.2 mg g-1, respectively.

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