In Situ Characterization of Ceria Oxidation States in High-Temperature Electrochemical Cells with Ambient Pressure XPS

2010 ◽  
Vol 114 (46) ◽  
pp. 19853-19861 ◽  
Author(s):  
Steven C. DeCaluwe ◽  
Michael E. Grass ◽  
Chunjuan Zhang ◽  
Farid El Gabaly ◽  
Hendrik Bluhm ◽  
...  
Keyword(s):  
High Temperature ◽  
Ambient Pressure ◽  
Oxidation States ◽  
Electrochemical Cells ◽  
In Situ Characterization ◽  
Ambient Pressure Xps

scholarly journals In Situ Characterization of Mesoporous Co/CeO2 Catalysts for the High-Temperature Water-Gas Shift

2018 ◽  
Vol 122 (16) ◽  
pp. 8998-9008 ◽  
Author(s):  
Dimitriy Vovchok ◽  
Curtis J. Guild ◽  
Shanka Dissanayake ◽  
Jordi Llorca ◽  
Eli Stavitski ◽  
...  
Keyword(s):  
High Temperature ◽  
Water Gas Shift ◽  
In Situ Characterization ◽  
High Temperature Water ◽  
Water Gas ◽  
Temperature Water

D-50 in Situ Characterization of High-Temperature Shift Catalysts

2007 ◽  
Vol 22 (2) ◽  
pp. 190-190
Author(s):  
A. M. Molenbroek ◽  
R. E. Johnsen ◽  
K. Sta˚hl
Keyword(s):  
High Temperature ◽  
Temperature Shift ◽  
In Situ Characterization

Exploiting In-Situ Characterization for a Sabatier Reaction to Reveal Catalytic Details

Chemistry ◽  
2021 ◽  
Vol 3 (4) ◽  
pp. 1157-1165
Author(s):  
Simon Yunes ◽  
Urim Pearl Kim ◽  
Hoang Nguyen ◽  
Jeffrey Kenvin
Keyword(s):  
High Temperature ◽  
Active Sites ◽  
Catalyst Deactivation ◽  
Active Species ◽  
Catalyst Characterization ◽  
In Situ Characterization ◽  
Spent Catalyst ◽  
Sabatier Reaction

In situ characterization of catalysts provides important information on the catalyst and the understanding of its activity and selectivity for a specific reaction. TPX techniques for catalyst characterization reveal the role of the support on the stabilization and dispersion of the active sites. However, these can be altered at high temperature since sintering of active species can occur as well as possible carbon deposition through the Bosch reaction, which hinders the active species and deactivates the catalyst. In situ characterization of the spent catalyst, however, may expose the causes for catalyst deactivation. For example, a simple TPO analysis on the spent catalyst may produce CO and CO2 via a reaction with O2 at high temperature and this is a strong indication that deactivation may be due to the deposition of carbon during the Sabatier reaction. Other TPX techniques such as TPR and pulse chemisorption are also valuable techniques when they are applied in situ to the fresh catalyst and then to the catalyst upon deactivation.

scholarly journals In situ characterization of the effects of Nb and Sn on the anatase–rutile transition in TiO2 nanotubes using high-temperature X-ray diffraction

2014 ◽  
Vol 307 ◽  
pp. 372-381 ◽  
Author(s):  
Nathália C. Verissimo ◽  
Alessandra Cremasco ◽  
Christiane A. Rodrigues ◽  
Rodnei Bertazzoli ◽  
Rubens Caram
Keyword(s):  
High Temperature ◽  
Tio2 Nanotubes ◽  
X Ray Diffraction ◽  
In Situ Characterization ◽  
X Ray

scholarly journals Enhanced Stability of Pt-Cu Single-Atom Alloy Catalysts: In Situ Characterization of the Pt/Cu(111) Surface in an Ambient Pressure of CO

2018 ◽  
Vol 122 (8) ◽  
pp. 4488-4495 ◽  
Author(s):  
Juan Pablo Simonovis ◽  
Adrian Hunt ◽  
Robert M. Palomino ◽  
Sanjaya D. Senanayake ◽  
Iradwikanari Waluyo
Keyword(s):  
Ambient Pressure ◽  
Single Atom ◽  
In Situ Characterization ◽  
Alloy Catalysts ◽  
Enhanced Stability ◽  
Single Atom Alloy

In situ characterization of surfaces at high temperature by using simultaneously a pyroreflectometer and an X-ray diffractometer

1998 ◽  
Vol 135 (1-4) ◽  
pp. 91-96 ◽  
Author(s):  
G. Llauro ◽  
D. Hernandez ◽  
F. Sibieude ◽  
J.M. Gineste ◽  
R. Verges ◽  
...  
Keyword(s):  
High Temperature ◽  
In Situ Characterization ◽  
X Ray

In Situ Characterization of a Nb and Mo Containingγ-TiAl Based Alloy Using Neutron Diffraction and High-Temperature Microscopy

2009 ◽  
Vol 11 (11) ◽  
pp. 932-937 ◽  
Author(s):  
Ian J. Watson ◽  
Klaus-Dieter Liss ◽  
Helmut Clemens ◽  
Wilfried Wallgram ◽  
Thomas Schmoelzer ◽  
...  
Keyword(s):  
High Temperature ◽  
Neutron Diffraction ◽  
In Situ Characterization
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