Synthesis of a Mycobacterium tuberculosis Tetra-acylated Sulfolipid Analogue and Characterization of the Chiral Acyl Chains Using Anisotropic NAD 2D-NMR Spectroscopy

2013 ◽  
Vol 78 (15) ◽  
pp. 7648-7657 ◽  
Author(s):  
Aurélie Lemétais ◽  
Yann Bourdreux ◽  
Philippe Lesot ◽  
Jonathan Farjon ◽  
Jean-Marie Beau
Keyword(s):  
Mycobacterium Tuberculosis ◽  
Nmr Spectroscopy ◽  
2D Nmr ◽  
2D Nmr Spectroscopy ◽  
Acyl Chains

scholarly journals Characterization of the Structure of 2-(4-methyl-2 Phenyl-4, 5-dihydrooxazol-4-ylmethyl)-isoindole-1, 3-dione by 1D, COSY and HSQC 2D NMR Spectroscopy

2021 ◽  
pp. 30-37
Author(s):  
Khadim Dioukhane ◽  
Younas Aouine ◽  
Asmae Nakkabi ◽  
Salaheddine Boukhssas ◽  
Hassane Faraj ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
2D Nmr ◽  
The Other ◽  
Two Dimensional ◽  
Hsqc Spectrum ◽  
2D Nmr Spectroscopy ◽  
Perfect Correlation ◽  
Dione Derivative ◽  
The One

The identity of the 2-(4-Methyl-2-phenyl-4,5-dihydrooxazol-4-ylmethyl)-isoindole-1,3-dione, previously synthesized in our laboratory, was proven without doubt by means of 1D and 2D NMR spectroscopy. Two-dimensional NMR spectroscopy played a major role. The analysis of the 2D-COSY spectrum of isoindoline-1,3-dione derivative shows a perfect correlation between neighboring protons. Thus, a correlation was noted between the protons of the phthalimide, H(8) and H(9) on the one hand and H(8') and H(9') on the other hand. The analysis of the 2D-HSQC spectrum of the studied compound indicates a faultless correlation between protons and adjacent carbons, and no correlation in the case of all quaternary carbons.

Characterization of epoxidized natural rubber by 2D NMR spectroscopy

Polymer ◽  
2007 ◽  
Vol 48 (3) ◽  
pp. 750-757 ◽  
Author(s):  
Takayuki Saito ◽  
Warunee Klinklai ◽  
Seiichi Kawahara
Keyword(s):  
Nmr Spectroscopy ◽  
Natural Rubber ◽  
2D Nmr ◽  
Epoxidized Natural Rubber ◽  
2D Nmr Spectroscopy

Rapid characterization of cocaine in illicit drug samples by 1D and 2D NMR spectroscopy

2018 ◽  
Vol 410 (21) ◽  
pp. 5237-5244 ◽  
Author(s):  
Mehdi Yemloul ◽  
I. Made Adyatmika ◽  
Stefano Caldarelli ◽  
Denis Ollivier ◽  
Mylène Campredon
Keyword(s):  
Nmr Spectroscopy ◽  
Illicit Drug ◽  
2D Nmr ◽  
2D Nmr Spectroscopy ◽  
Rapid Characterization
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