Determination of enantiomeric purity of chiral lactones. A general method using nuclear magnetic resonance

Ignac J. Jakovac; J. Bryan Jones

doi:10.1021/jo01327a028

Determination of enantiomeric purity of chiral lactones. A general method using nuclear magnetic resonance

The Journal of Organic Chemistry ◽

10.1021/jo01327a028 ◽

1979 ◽

Vol 44 (13) ◽

pp. 2165-2168 ◽

Cited By ~ 40

Author(s):

Ignac J. Jakovac ◽

J. Bryan Jones

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Enantiomeric Purity ◽

Chiral Lactones ◽

General Method ◽

Nuclear Magnetic

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ChemInform Abstract: DETERMINATION OF ENANTIOMERIC PURITY OF CHIRAL LACTONES. A GENERAL METHOD USING NUCLEAR MAGNETIC RESONANCE

Chemischer Informationsdienst ◽

10.1002/chin.197942074 ◽

1979 ◽

Vol 10 (42) ◽

Author(s):

I. J. JAKOVAC ◽

J. B. JONES

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Enantiomeric Purity ◽

Chiral Lactones ◽

General Method ◽

Nuclear Magnetic

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Determination of enantiomeric purity and absolute configuration of chiral β-propiolactones by nuclear magnetic resonance in optically active solvents.

Tetrahedron Letters ◽

10.1016/s0040-4039(00)81594-4 ◽

1983 ◽

Vol 24 (10) ◽

pp. 1027-1030 ◽

Cited By ~ 13

Author(s):

Alain Leborgne ◽

Michel Moreau ◽

Nicolas Spassky

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Optically Active ◽

Nuclear Magnetic

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ChemInform Abstract: DETERMINATION OF THE ENANTIOMERIC PURITY OF ISOQUINOLINE ALKALOIDS BY THE USE OF CHIRAL LANTHANIDE NUCLEAR MAGNETIC RESONANCE SHIFT REAGENTS

Chemischer Informationsdienst ◽

10.1002/chin.197542452 ◽

1975 ◽

Vol 6 (42) ◽

Author(s):

N. A. SHAATH ◽

T. O. SOINE

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Enantiomeric Purity ◽

Isoquinoline Alkaloids ◽

Resonance Shift ◽

Shift Reagents ◽

Nuclear Magnetic Resonance Shift ◽

Nuclear Magnetic

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ChemInform Abstract: PROTON AND DEUTERIUM NUCLEAR MAGNETIC RESONANCE DETERMINATION OF THE ENANTIOMERIC PURITY AND ABSOLUTE CONFIGURATION OF α-DEUTERATED PRIMARY CARBOXYLIC ACIDS, ALCOHOLS, AND AMINES

Chemischer Informationsdienst ◽

10.1002/chin.198315084 ◽

1983 ◽

Vol 14 (15) ◽

Author(s):

D. PARKER

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Carboxylic Acids ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Nuclear Magnetic

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ChemInform Abstract: THE USE OF CHIRAL SOLVATING AGENT FOR NUCLEAR MAGNETIC RESONANCE DETERMINATION OF ENANTIOMERIC PURITY AND ABSOLUTE CONFIGURATION OF LACTONES. CONSEQUENCES OF THREE-POINT INTERACTIONS

Chemischer Informationsdienst ◽

10.1002/chin.197733058 ◽

1977 ◽

Vol 8 (33) ◽

pp. no-no

Author(s):

W. H. PIRKLE ◽

D. L. SIKKENGA

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Point Interactions ◽

Chiral Solvating Agent ◽

Nuclear Magnetic

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ChemInform Abstract: CHIRAL NUCLEAR MAGNETIC RESONANCE SOLVATING AGENTS. RESOLUTION, DETERMINATION OF ENANTIOMERIC PURITY, AND ASSIGNMENT OF ABSOLUTE CONFIGURATION OF CYCLIC AND ACYCLIC SULFINATE ESTERS

Chemischer Informationsdienst ◽

10.1002/chin.197625117 ◽

1976 ◽

Vol 7 (25) ◽

pp. no-no

Author(s):

WILLIAM H. PIRKLE ◽

MARVIN S. HOEKSTRA

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Sulfinate Esters ◽

Nuclear Magnetic

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The use of chiral solvating agent for nuclear magnetic resonance determination of enantiomeric purity and absolute configuration of lactones. Consequences of three-point interactions

The Journal of Organic Chemistry ◽

10.1021/jo00428a023 ◽

1977 ◽

Vol 42 (8) ◽

pp. 1370-1374 ◽

Cited By ~ 78

Author(s):

William H. Pirkle ◽

David L. Sikkenga

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Point Interactions ◽

Chiral Solvating Agent ◽

Nuclear Magnetic

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Chiral nuclear magnetic resonance solvating agents. Resolution, determination of enantiomeric purity, and assignment of absolute configuration of cyclic and acyclic sulfinate esters

Journal of the American Chemical Society ◽

10.1021/ja00423a031 ◽

1976 ◽

Vol 98 (7) ◽

pp. 1832-1839 ◽

Cited By ~ 71

Author(s):

William H. Pirkle ◽

Marvin S. Hoekstra

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Absolute Configuration ◽

Enantiomeric Purity ◽

Sulfinate Esters ◽

Nuclear Magnetic

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Determination of the enantiomeric purity of isoquinoline alkaloids by the use of chiral lanthanide nuclear magnetic resonance shift reagents

The Journal of Organic Chemistry ◽

10.1021/jo00901a025 ◽

1975 ◽

Vol 40 (13) ◽

pp. 1987-1988 ◽

Cited By ~ 10

Author(s):

Nadim A. Shaath ◽

Taito O. Soine

Keyword(s):

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Enantiomeric Purity ◽

Isoquinoline Alkaloids ◽

Resonance Shift ◽

Shift Reagents ◽

Nuclear Magnetic Resonance Shift ◽

Nuclear Magnetic

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1H-nuclear magnetic resonance determination of the enantiomeric purity of aliphatic primary amines, β-aminoalcohols, β-diamines and α-amino-acids with 1R-(−)-myrtenal: scope and limitations

Spectrochimica Acta Part A Molecular and Biomolecular Spectroscopy ◽

10.1016/s1386-1425(02)00305-0 ◽

2003 ◽

Vol 59 (6) ◽

pp. 1239-1245 ◽

Cited By ~ 20

Author(s):

François Dufrasne ◽

Michel Gelbcke ◽

Jean Nève

Keyword(s):

Amino Acids ◽

Nuclear Magnetic Resonance ◽

Magnetic Resonance ◽

Enantiomeric Purity ◽

Primary Amines ◽

1H Nuclear Magnetic Resonance ◽

Nuclear Magnetic

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