Aroma Compounds from Aqueous Solution of Haze (Rhus succedanea) Honey Determined by Adsorptive Column Chromatography

1996 ◽  
Vol 44 (12) ◽  
pp. 3913-3918 ◽  
Author(s):  
Mitsuya Shimoda ◽  
Yin Wu ◽  
Yutaka Osajima
Keyword(s):  
Aqueous Solution ◽  
Column Chromatography ◽  
Aroma Compounds ◽  
Rhus Succedanea

Colorimetric Determination of Oxyphenisatin and Oxyphenisatin Diacetate in Pharmaceutical Preparations

1964 ◽  
Vol 47 (4) ◽  
pp. 688-692
Author(s):  
Antoine Major
Keyword(s):  
Aqueous Solution ◽  
Organic Solvent ◽  
Silver Nitrate ◽  
Sodium Hydroxide ◽  
Column Chromatography ◽  
Sodium Hydroxide Solution ◽  
Pharmaceutical Preparations ◽  
Colorimetric Determination ◽  
Hydroxide Solution

Abstract A method is described which will quantitatively determine 0.1 mg oxyphenisatin or the diacetate in various pharmaceutical preparations. After removal of interferences by organic solvent extractions from aqueous solution and partition column chromatography, the reaction of oxyphenisatin (diacetate) with silver nitrate in alcoholic sodium hydroxide solution produces a violet solution, which follows Beer’s law (1—15 μg per ml). The method was satisfactorily applied to the assay of commercial tablets, liquids, and powders with recoveries, as per cent found of declared, in the range 95—101%.

Strahlenchemie von Kohlenhydraten, IV. γ-Radiolyse von Cellobiose in N2O-gesättigter wäßriger Lösung / γ-Radiolysis of Cellobiose in N2O Saturated Aqueous Solution

1973 ◽  
Vol 28 (9-10) ◽  
pp. 635-646 ◽  
Author(s):  
Miral Dizdaroglu ◽  
Clemens Von Sonntag
Keyword(s):  
Aqueous Solution ◽  
Aqueous Solutions ◽  
Column Chromatography ◽  
Gluconic Acid ◽  
Analytical Techniques ◽  
Saturated Aqueous Solution ◽  
Hydroxymethyl Furfural ◽  
Cellobionic Acid

After γ-radiolysis of N2O saturated deoxygenated aqueous solutions of cellobiose (10-2Μ) the following products have been determined: Glucose, gluconic acid, 5-keto-glucose, 4-deoxy-glucose, 5-deoxy-gluconic acid, 2-deoxy-gluconic acid, 3-deoxy-4-keto-glucose, 2-deoxy-5-keto-glucose, 4-deoxy-5-keto-glucose, arabinose, 2-deoxy-ribose, ribose, erythrose, threose, 2-deoxy-tetrose, dihydroxy acetone, 3-deoxy-pentulose, 2-butanone-1,4-diol, 5-hydroxymethyl-furfural, carbon monoxid, and C12-acids (probably cellobionic acid and 2-deoxy-cellobionic acid). Analytical techniques were column chromatography, t. l. c. and g. l. c. combined with m. s.

Furazolidone and Nitrofurazone in Feeds

1966 ◽  
Vol 49 (2) ◽  
pp. 325-328
Author(s):  
Loyal R Stone
Keyword(s):  
Aqueous Solution ◽  
Aluminum Oxide ◽  
Rapid Method ◽  
Column Chromatography ◽  
Collaborative Studies

Abstract Collaborative studies were continued on a rapid method for furazolidone in feeds where the drug is isolated by column chromatography and measured in aqueous solution. This procedure was extended to determine both furazolidone and nitrofurazone separately in feeds medicated with bifuran and was studied collaboratively. The activity of the aluminum oxide adsorbent in these procedures is critical. However, with a suitable lot of adsorbent, these proposed procedures are more rapid and specific than the official methods.

HTPB-based polyurethaneurea membranes for recovery of aroma compounds from aqueous solution by pervaporation

2007 ◽  
Vol 104 (1) ◽  
pp. 552-559 ◽  
Author(s):  
Yunxiang Bai ◽  
Jinwen Qian ◽  
Jian Yin ◽  
Zhibin Zhai ◽  
Yang Yang
Keyword(s):  
Aqueous Solution ◽  
Aroma Compounds

Retention of aroma compounds by proteins in aqueous solution

1995 ◽  
Vol 54 (4) ◽  
pp. 387-392 ◽  
Author(s):  
P. Landy ◽  
C. Druaux ◽  
A. Voilley
Keyword(s):  
Aqueous Solution ◽  
Aroma Compounds

Structures Formed by Cryoprotective Agents Used in Freezc-Etching

1971 ◽  
Vol 29 ◽  
pp. 448-449
Author(s):  
G. G. Cocks ◽  
C. E. Cluthe
Keyword(s):  
Aqueous Solution ◽  
Polyethylene Oxide ◽  
Liquid Nitrogen Temperature ◽  
Ice Crystals ◽  
Etching Technique ◽  
Structural Constituent ◽  
Cryoprotective Agents ◽  
Quick Freezing ◽  
Freeze Etching ◽  
Fractured Surface

The freeze etching technique is potentially useful for examining dilute solutions or suspensions of macromolecular materials. Quick freezing of aqueous solutions in Freon or propane at or near liquid nitrogen temperature produces relatively large ice crystals and these crystals may damage the structures to be examined. Cryoprotective agents may reduce damage to the specimem, hut their use often results in the formation of a different set of specimem artifacts.In a study of the structure of polyethylene oxide gels glycerol and sucrose were used as cryoprotective agents. The experiments reported here show some of the structures which can appear when these cryoprotective agents are used.Figure 1 shows a fractured surface of a frozen 25% aqueous solution of sucrose. The branches of dendritic ice crystals surrounded hy ice-sucrose eutectic can be seen. When this fractured surface is etched the ice in the dendrites sublimes giving the type of structure shown in Figure 2. The ice-sucrose eutectic etches much more slowly. It is the smooth continuous structural constituent surrounding the branches of the dendrites.

Preparation and characterisation of vanadium pentoxide supported rhodium catalyst

1988 ◽  
Vol 46 ◽  
pp. 946-947
Author(s):  
A. Legrouri
Keyword(s):  
Aqueous Solution ◽  
Thermal Decomposition ◽  
Physicochemical Properties ◽  
Surface Area ◽  
Vanadium Pentoxide ◽  
High Purity ◽  
Gas Adsorption ◽  
Rhodium Catalyst ◽  
Optical Methods ◽  
Reducible Oxides

The industrial importance of metal catalysts supported on reducible oxides has stimulated considerable interest during the last few years. This presentation reports on the study of the physicochemical properties of metallic rhodium supported on vanadium pentoxide (Rh/V2O5). Electron optical methods, in conjunction with other techniques, were used to characterise the catalyst before its use in the hydrogenolysis of butane; a reaction for which Rh metal is known to be among the most active catalysts.V2O5 powder was prepared by thermal decomposition of high purity ammonium metavanadate in air at 400 °C for 2 hours. Previous studies of the microstructure of this compound, by HREM, SEM and gas adsorption, showed it to be non— porous with a very low surface area of 6m2/g3. The metal loading of the catalyst used was lwt%Rh on V2Q5. It was prepared by wet impregnating the support with an aqueous solution of RhCI3.3H2O.

TEM observation of iron oxide pillars in montmorillonite

1990 ◽  
Vol 48 (4) ◽  
pp. 882-883
Author(s):  
H. Mori ◽  
Y. Murata ◽  
H. Yoneyama ◽  
H. Fujita
Keyword(s):  
Aqueous Solution ◽  
Iron Oxide ◽  
Fine Particles ◽  
Aqueous Suspension ◽  
Volume Ratio ◽  
Exchange Capacity ◽  
Nano Composites ◽  
Pillared Montmorillonite ◽  
Topographic Features ◽  
Transmission Electron

Recently, a new sort of nano-composites has been prepared by incorporating such fine particles as metal oxide microcrystallites and organic polymers into the interlayer space of montmorillonite. Owing to their extremely large specific surface area, the nano-composites are finding wide application[1∼3]. However, the topographic features of the microstructures have not been elucidated as yet In the present work, the microstructures of iron oxide-pillared montmorillonite have been investigated by high-resolution transmission electron microscopy.Iron oxide-pillared montmorillonite was prepared through the procedure essentially the same as that reported by Yamanaka et al. Firstly, 0.125 M aqueous solution of trinuclear acetato-hydroxo iron(III) nitrate, [Fe3(OCOCH3)7 OH.2H2O]NO3, was prepared and then the solution was mixed with an aqueous suspension of 1 wt% clay by continuously stirring at 308 K. The final volume ratio of the latter aqueous solution to the former was 0.4. The clay used was sodium montmorillonite (Kunimine Industrial Co.), having a cation exchange capacity of 100 mequiv/100g. The montmorillonite in the mixed suspension was then centrifuged, followed by washing with deionized water. The washed samples were spread on glass plates, air dried, and then annealed at 673 K for 72 ks in air. The resultant film products were approximately 20 μm in thickness and brown in color.

The microstructure of functionalized poLyacrylonitrile beads for bioseparations

1990 ◽  
Vol 48 (4) ◽  
pp. 1094-1095
Author(s):  
Eduardo A. Kamenetzky ◽  
David A. Ley
Keyword(s):  
Aqueous Solution ◽  
Affinity Chromatography ◽  
Pore Size Distribution ◽  
Pore Size ◽  
Surface Coverage ◽  
Vacuum Impregnation ◽  
Thin Sections ◽  
Selective Staining ◽  
Low Viscosity ◽  
Diamond Knife

The microstructure of polyacrylonitrile (PAN) beads for affinity chromatography bioseparations was studied by TEM of stained ultramicrotomed thin-sections. Microstructural aspects such as overall pore size distribution, the distribution of pores within the beads, and surface coverage of functionalized beads affect performance properties. Stereological methods are used to quantify the internal structure of these chromatographic supports. Details of the process for making the PAN beads are given elsewhere. TEM specimens were obtained by vacuum impregnation with a low-viscosity epoxy and sectioning with a diamond knife. The beads can be observed unstained. However, different surface functionalities can be made evident by selective staining. Amide surface coverage was studied by staining in vapor of a 0.5.% RuO4 aqueous solution for 1 h. RuO4 does not stain PAN but stains, amongst many others, polymers containing an amide moiety.

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