Ochratoxin A Determination in Beer by Solid-Phase Microextraction Coupled to Liquid Chromatography with Fluorescence Detection:  A Fast and Sensitive Method for Assessment of Noncompliance to Legal Limits

2006 ◽  
Vol 54 (5) ◽  
pp. 1594-1598 ◽  
Author(s):  
Antonella Aresta ◽  
Francesco Palmisano ◽  
Rosa Vatinno ◽  
Carlo G. Zambonin
Keyword(s):  
Liquid Chromatography ◽  
Ochratoxin A ◽  
Fluorescence Detection ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Legal Limits ◽  
Sensitive Method

A sensitive method to determine melatonin in saliva by automated online in-tube solid-phase microextraction coupled with stable isotope-dilution liquid chromatography-tandem mass spectrometry

2017 ◽  
Vol 9 (21) ◽  
pp. 3134-3140 ◽  
Author(s):  
Atsushi Ishizaki ◽  
Akiko Uemura ◽  
Hiroyuki Kataoka
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Stable Isotope ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Tandem Mass ◽  
Stable Isotope Dilution ◽  
Chromatography Tandem Mass Spectrometry ◽  
Liquid Chromatography Tandem Mass ◽  
Sensitive Method

Melatonin (MLT) plays important roles in regulating the sleep-wake cycle, and has many beneficial effects on health. A simple, rapid, and sensitive method was developed for the determination of MLT in human saliva by automated online in-tube solid-phase microextraction coupled with stable isotope-dilution liquid chromatography-tandem mass spectrometry.

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