Matrix Solid-Phase Dispersion Extraction and Gas Chromatographic Determination of Chloramphenicol in Muscle Tissue

2003 ◽  
Vol 51 (4) ◽  
pp. 871-875 ◽  
Author(s):  
Helena Kubala-Drincic ◽  
Davorin Bazulic ◽  
Jasenka Sapunar-Postruznik ◽  
Mirela Grubelic ◽  
Goran Stuhne
Keyword(s):  
Muscle Tissue ◽  
Solid Phase ◽  
Chromatographic Determination ◽  
Matrix Solid Phase Dispersion ◽  
Phase Dispersion

Matrix Solid-Phase Dispersion Isolation and Liquid Chromatographic Determination of Oxolinic Acid in Channel Catfish (Ictalurus punctatus) Muscle Tissue

1992 ◽  
Vol 75 (3) ◽  
pp. 428-432 ◽  
Author(s):  
Herman H Jarboe ◽  
Kevin M Kleinow
Keyword(s):  
Muscle Tissue ◽  
Ictalurus Punctatus ◽  
Channel Catfish ◽  
Solid Phase ◽  
Chromatographic Determination ◽  
Oxolinic Acid ◽  
Matrix Solid Phase Dispersion ◽  
Phase Dispersion ◽  
Liquid Chromatographic Determination ◽  
Liquid Chromatographic

Abstract Matrix solid-phase dispersion Isolation and liquid chromatographic techniques were developed to quantify oxolinic acid (OA) and OA-related metabolites in channel catfish (Ictalurus punctatus) muscle tissue and bile. Mean percent recovery, correlation coefficient, and inter- and intra-assay variabilities were 82.8 ±15.0%, 0.996 ±0.004,12.5 ±8.9%, and 1.22%, respectively, for OA Isolated from fortified muscle tissue. Using the methodologies described in the current study, incurred OA In muscle tissue and 4 OA-related metabolites were Isolated In the bile of dosed catfish.

Sign in / Sign up

Export Citation Format

Share Document