Detection of Electrochemical Reaction Products from the Sodium–Oxygen Cell with Solid-State 23Na NMR Spectroscopy

2017 ◽  
Vol 139 (2) ◽  
pp. 595-598 ◽  
Author(s):  
Zoë E. M. Reeve ◽  
Christopher J. Franko ◽  
Kristopher J. Harris ◽  
Hossein Yadegari ◽  
Xueliang Sun ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Electrochemical Reaction ◽  
Reaction Products ◽  
23Na Nmr

Solid-state 23Na NMR spectroscopy studies of ordered and disordered cellulose nanocrystal films

2019 ◽  
Vol 97 ◽  
pp. 31-39 ◽  
Author(s):  
Ryutaro Ohashi ◽  
Carl A. Michal ◽  
Wadood Y. Hamad ◽  
Thanh-Dinh Nguyen ◽  
Motohiro Mizuno ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Cellulose Nanocrystal ◽  
Nanocrystal Films ◽  
Spectroscopy Studies ◽  
23Na Nmr

scholarly journals A Simple and Efficient Mechanochemical Route for the Synthesis of Salophen Ligands and of the Corresponding Zn, Ni, and Pd Complexes

Molecules ◽  
2019 ◽  
Vol 24 (12) ◽  
pp. 2314 ◽  
Author(s):  
Luca Leoni ◽  
Andrea Carletta ◽  
Luca Fusaro ◽  
Jean Dubois ◽  
Nikolay A. Tumanov ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Single Crystal ◽  
Solid State Nmr ◽  
Good Alternative ◽  
Reaction Products ◽  
X Ray Diffraction ◽  
One Pot ◽  
X Ray ◽  
Pd Complexes

A number of salophen ligands and their Zn, Ni, and Pd complexes were synthesized by an efficient one-pot mechanosynthesis protocol. The reaction products were characterized by means of complementary solid-state techniques, i.e., powder X-ray diffraction, single-crystal X-ray diffraction, and solid-state NMR spectroscopy. Four new crystal structures of metal salophen complexes as DMSO solvates are here reported. The described simple and relatively fast (about 1 h for all derivatives) procedure is a good alternative to classical methods performed in organic solvents.

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