scholarly journals Ultrafast Electron Diffraction Tomography for Structure Determination of the New Zeolite ITQ-58

2016 ◽  
Vol 138 (32) ◽  
pp. 10116-10119 ◽  
Author(s):  
Jorge Simancas ◽  
Raquel Simancas ◽  
Pablo J. Bereciartua ◽  
Jose L. Jorda ◽  
Fernando Rey ◽  
...  
2017 ◽  
Vol 85 ◽  
pp. 110-116 ◽  
Author(s):  
Mariana Klementová ◽  
Miroslav Karlík ◽  
Pavel Novák ◽  
Lukáš Palatinus

2019 ◽  
Vol 25 (S2) ◽  
pp. 2450-2451
Author(s):  
Mariana Klementova ◽  
Lukas Palatinus ◽  
Jörg Fritz ◽  
Ansgar Greshake ◽  
Richard Wirth ◽  
...  

2018 ◽  
Vol 57 (16) ◽  
pp. 10241-10248 ◽  
Author(s):  
Enrico Mugnaioli ◽  
Mauro Gemmi ◽  
Renyong Tu ◽  
Jeremy David ◽  
Giovanni Bertoni ◽  
...  

2018 ◽  
Vol 4 (12) ◽  
pp. eaau6178 ◽  
Author(s):  
Péter Németh ◽  
Enrico Mugnaioli ◽  
Mauro Gemmi ◽  
György Czuppon ◽  
Attila Demény ◽  
...  

Despite its thermodynamical metastability at near-surface conditions, aragonite is widespread in marine and terrestrial sediments. It abundantly forms in living organisms, and its abiotic formation is favored in waters of a Mg2+/Ca2+ratio > 1.5. Here, we provide crystallographic evidence of a nanocrystalline CaCO3polymorph, which precipitates before aragonite in a cave. The new phase, which we term monoclinic aragonite (mAra), is crystallographically related to ordinary, orthorhombic aragonite. Electron diffraction tomography combined with structure determination demonstrates that mAra has a layered aragonite structure, in which some carbonates can be replaced by hydroxyls and up to 10 atomic % of Mg can be incorporated. The diagnostic electron diffraction features of mAra are diffuse scattering and satellite reflections along aragonite {110}. Similar features have previously been reported—although unrecognized—from biogenic aragonite formed in stromatolites, mollusks, and cyanobacteria as well as from synthetic material. We propose that mAra is a widespread crystalline CaCO3that plays a hitherto unrecognized key role in metastable aragonite formation.


2016 ◽  
Vol 3 (11) ◽  
pp. 1351-1362 ◽  
Author(s):  
Zhengyang Zhou ◽  
Lukáš Palatinus ◽  
Junliang Sun

The combination of PXRD and ED is applied to determine modulated structures which resist solution by more conventional methods.


1969 ◽  
Vol 23 ◽  
pp. 3224-3234 ◽  
Author(s):  
B. Andersen ◽  
H. M. Seip ◽  
T. G. Strand ◽  
R. Stølevik ◽  
Gunner Borch ◽  
...  

2017 ◽  
Vol 4 (10) ◽  
pp. 1654-1659 ◽  
Author(s):  
Yilin Wang ◽  
Yunchen Wang ◽  
Jie Su ◽  
Xiaowei Song ◽  
Wei Wan ◽  
...  

Structure determination of silicogermanate with sti layers pillared by D4R/Ge7 units by rotation electron diffraction and powder X-ray diffraction.


Sign in / Sign up

Export Citation Format

Share Document