Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

2016 ◽  
Vol 138 (22) ◽  
pp. 7121-7129 ◽  
Author(s):  
Gregory Morrison ◽  
Mark D. Smith ◽  
Hans-Conrad zur Loye
Keyword(s):  
Flux Growth ◽  
Growth Method ◽  
Uranyl Silicates

Synthesis, Structure and Magnetism of ErCoIn5

2004 ◽  
Vol 848 ◽  
Author(s):  
Evan Lyle Thomas ◽  
Erin E. Erickson ◽  
Monica Moldovan ◽  
David P. Young ◽  
Julia Y. Chan
Keyword(s):  
Magnetic Properties ◽  
Electrical Resistivity ◽  
Magnetic Susceptibility ◽  
Single Crystal ◽  
Experimental Results ◽  
Flux Growth ◽  
X Ray Diffraction ◽  
Metallic Behavior ◽  
X Ray ◽  
Growth Method

AbstractA new member of the LnMIn5 family, ErCoIn5, has been synthesized by a flux-growth method. The structure of ErCoIn5 was determined by single crystal X-ray diffraction. It crystallizes in the tetragonal space group P4/mmm, Z = 1, with lattice parameters a = 4.5400(4) and c = 7.3970(7) Å, and V = 152.46(2) Å3. Electrical resistivity data show metallic behavior. Magnetic susceptibility measurements show this compound to be antiferromagnetic with TN = 5.1 K. We compare these experimental results with those of LaCoIn5 in an effort to better understand the effect of the structural trends observed on the transport and magnetic properties.

Crystal structure determination of non-stoichiometric Ca4−xRuO6−x (x = 1.17) from X-ray powder diffraction data

2016 ◽  
Vol 31 (1) ◽  
pp. 59-62
Author(s):  
Martin Etter ◽  
Maximilian J. Krautloher ◽  
Nakheon Sung ◽  
Joel Bertinshaw ◽  
Bumjoon Kim ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Powder Diffraction ◽  
Flux Growth ◽  
Powder Diffraction Data ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Growth Method ◽  
Calcium Ruthenate

A new non-stoichiometric calcium ruthenate [Ca4−xRuO6−x with x = 1.17(1)] was synthesized by the flux growth method and characterized by the X-ray powder diffraction. The crystal structure is isostructural to the K4CdCl6 type with space group R$\bar 3$c. Unit-cell parameters are a = 9.2881(1), c = 11.1634(2) Å, V = 834.03(3) Å3, and Z = 6.

scholarly journals The Influence of Growth Rate on Porosity in Al-Pd-Mn Icosahedral Quasicrystals.

2000 ◽  
Vol 643 ◽  
Author(s):  
Amy R. Ross ◽  
Ian R. Fisher ◽  
Paul C. Canfield ◽  
Thomas A. Lograsso
Keyword(s):  
Growth Rate ◽  
Crystal Size ◽  
Growth Conditions ◽  
Flux Growth ◽  
Local Growth ◽  
Cooling Rates ◽  
Porosity Level ◽  
Growth Method ◽  
Icosahedral Quasicrystals ◽  
Growth Experiments

AbstractGrowth experiments have been carried out to characterize the occurrence and development of porosity in Bridgman and flux grown Al-Pd-Mn icosahedral quasicrystals. The porosity level has been observed to fluctuate between values of 0.0 and 3.75 percent along the length of Bridgman single crystals implying that the development of porosity is affected by the local growth conditions. Experiments were conducted to evaluate the influence of the rate of solidification on the occurrence of porosity. Alloys were solidified with different growth rates, 1mm/hr and >10 mm/hr, using the Bridgman configuration and at different cooling rates, ranging from 0.29°C/hr to 10°C/hr, using the flux growth method. Porosity levels were analyzed via optical image analysis. These experiments indicate that porosity percentages are greatly influenced by cooling rates and crystal size.

Growth, mechanical and domain structure studies of Na0.5Bi0.5TiO3 single crystal grown by flux growth method

2017 ◽  
Vol 721 ◽  
pp. 199-204 ◽  
Author(s):  
P. Ramesh Babu ◽  
Rachna Selvamani ◽  
Gurvinderjit Singh ◽  
S. Kalainathan ◽  
Ravishanker Babu ◽  
...  
Keyword(s):  
Single Crystal ◽  
Domain Structure ◽  
Flux Growth ◽  
Growth Method

scholarly journals Synthesis of trace element bearing single crystals of Chlor-Apatite (Ca5(PO4)3Cl) using the flux growth method

2013 ◽  
Vol 7 (1) ◽  
Author(s):  
Stephan Klemme ◽  
Timm John ◽  
Mathias Wessels ◽  
Christof Kusebauch ◽  
Jasper Berndt ◽  
...  
Keyword(s):  
Trace Element ◽  
Single Crystals ◽  
Flux Growth ◽  
Growth Method ◽  
Element Bearing

Fabrication of La2Ti2O7 Crystals Using an Alkali-Metal Molybdate Flux Growth Method and Their Nitridability To Form LaTiO2N Crystals under a High-Temperature NH3 Atmosphere

2015 ◽  
Vol 54 (7) ◽  
pp. 3237-3244 ◽  
Author(s):  
Mirabbos Hojamberdiev ◽  
Akiko Yamaguchi ◽  
Kunio Yubuta ◽  
Shuji Oishi ◽  
Katsuya Teshima
Keyword(s):  
High Temperature ◽  
Alkali Metal ◽  
Flux Growth ◽  
Metal Molybdate ◽  
Growth Method

Effect of Fe content on Cu2Fe x Zn1−x SnS4 single crystals fabricated by flux growth method

2018 ◽  
Vol 51 (29) ◽  
pp. 295107 ◽  
Author(s):  
Jun Zhang ◽  
Jun Liao ◽  
Lexi Shao ◽  
Shuwen Xue ◽  
Zhiguo Wang
Keyword(s):  
Single Crystals ◽  
Flux Growth ◽  
Fe Content ◽  
Growth Method
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