Determination of the Complete Structure of a Uniformly Labeled Molecule by Rotational Resonance Solid-State NMR in the Tilted Rotating Frame

1999 ◽  
Vol 121 (16) ◽  
pp. 4064-4065 ◽  
Author(s):  
Kaoru Nomura ◽  
K. Takegoshi ◽  
Takehiko Terao ◽  
Kenichi Uchida ◽  
Masatsune Kainosho
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Rotating Frame ◽  
Complete Structure ◽  
Rotational Resonance

Determination of Internuclear Distances in Uniformly Labeled Molecules by Rotational-Resonance Solid-State NMR

2003 ◽  
Vol 125 (9) ◽  
pp. 2718-2722 ◽  
Author(s):  
Philip T. F. Williamson ◽  
Aswin Verhoeven ◽  
Matthias Ernst ◽  
Beat H. Meier
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Rotational Resonance ◽  
Internuclear Distances

scholarly journals Structure determination of molecular nanocomposites by combining pair distribution function analysis and solid-state NMR

RSC Advances ◽  
2015 ◽  
Vol 5 (12) ◽  
pp. 8895-8902 ◽  
Author(s):  
E.-E. Bendeif ◽  
A. Gansmuller ◽  
K.-Y. Hsieh ◽  
S. Pillet ◽  
Th. Woike ◽  
...  
Keyword(s):  
Distribution Function ◽  
Solid State ◽  
Solid State Nmr ◽  
Pair Distribution Function ◽  
Function Analysis ◽  
Structural Characterisation ◽  
Atomic Pair Distribution Function ◽  
X Ray Scattering ◽  
Atomic Pair

Total X-ray scattering coupled to atomic pair distribution function analysis (PDF) and solid state NMR allowed the identification and structural characterisation of isolated molecules and nanocrystals of sodium nitroprusside confined in mesoporous silica.

Solid-State NMR Structure Determination of Whole Anchoring Threads from the Blue Mussel Mytilus edulis

2012 ◽  
Vol 14 (1) ◽  
pp. 132-141 ◽  
Author(s):  
Alexandre A. Arnold ◽  
Frédéric Byette ◽  
Marc-Olivier Séguin-Heine ◽  
André LeBlanc ◽  
Lekha Sleno ◽  
...  
Keyword(s):  
Solid State ◽  
Mytilus Edulis ◽  
Structure Determination ◽  
Solid State Nmr ◽  
Blue Mussel ◽  
Nmr Structure ◽  
Nmr Structure Determination

Rotational resonance in a spin-lock field for solid state NMR

1990 ◽  
Vol 168 (3-4) ◽  
pp. 304-308 ◽  
Author(s):  
Zhe-Hong Gan ◽  
David M. Grant
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Spin Lock ◽  
Rotational Resonance

scholarly journals Multidimensional high-resolution solid-state NMR for the structure determination of ^C/^N-labeled biomolecules

2000 ◽  
Vol 40 (supplement) ◽  
pp. S174
Author(s):  
Y. Todokoro ◽  
H. Yanagishita ◽  
T. Fujiwara ◽  
H. Akutsu
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Structure Determination ◽  
Solid State Nmr

Determination of the charge of Al13 Keggin oligocations intercalated into synthetic hectorite

2019 ◽  
Vol 74 (1) ◽  
pp. 85-90
Author(s):  
Marius Schöttle ◽  
Dominik Schuchardt ◽  
Andreas Edenharter ◽  
Sebastian Koch ◽  
Jürgen Senker ◽  
...  
Keyword(s):  
Reaction Time ◽  
Solid State ◽  
Ir Spectroscopy ◽  
Cation Exchange ◽  
Elemental Analysis ◽  
Crystalline Phase ◽  
Solid State Nmr ◽  
Liquid Crystalline ◽  
A Charge

AbstractApplying a nematic liquid crystalline phase of a synthetic Na-hectorite with layer separations >100 nm, the reaction time for pillaring with Al13 Keggin oligocation could be reduced to seconds ensuring that cation exchange is controlled by thermodynamics. With this material at hand we are able to resolve the long-standing dispute regarding the charge of intercalated Keggin oligocations. Micropore sizes as determined by physisorption isotherms, adsorption isotherms obtained via elemental analysis, and results of 27Al solid-state NMR and pyridine probe IR spectroscopy favor a charge of +7 for the Al13 pillars intercalated into hectorite unaltered.

Solid-state NMR at natural isotopic abundance for the determination of conformational polymorphism – the case of designed β-turn peptides containing di-prolines

2017 ◽  
Vol 53 (7) ◽  
pp. 1317-1320 ◽  
Author(s):  
Jayasubba Reddy Yarava ◽  
Rajesh Sonti ◽  
K. Kantharaju ◽  
S. Raghothama ◽  
K. V. Ramanathan
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Solution Nmr ◽  
Isotopic Abundance ◽  
Conformational Polymorphism ◽  
Natural Isotopic Abundance

Like nOe in solution NMR, through-space proton correlations have been exploited in the solid state to obtain the cis–trans conformational polymorphism.

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