Efficient Multispin Homonuclear Double-Quantum Recoupling for Magic-Angle Spinning NMR: 13C−13C Correlation Spectroscopy of U-13C-Erythromycin A

1998 ◽  
Vol 120 (41) ◽  
pp. 10602-10612 ◽  
Author(s):  
Chad M. Rienstra ◽  
Mary E. Hatcher ◽  
Leonard J. Mueller ◽  
Sun ◽  
Stephen W. Fesik ◽  
...  
Keyword(s):  
Magic Angle Spinning ◽  
Correlation Spectroscopy ◽  
Double Quantum ◽  
Magic Angle ◽  
Erythromycin A ◽  
Angle Spinning

scholarly journals Double-quantum filtered heteronuclear correlation spectroscopy under magic angle spinning

2007 ◽  
Vol 31 (1) ◽  
pp. 55-61 ◽  
Author(s):  
Yao-Hung Tseng ◽  
Yi-Ling Tsai ◽  
Tim W.T . Tsai ◽  
Chun-Pin Lin ◽  
Shih-Hao Huang ◽  
...  
Keyword(s):  
Magic Angle Spinning ◽  
Correlation Spectroscopy ◽  
Double Quantum ◽  
Magic Angle ◽  
Heteronuclear Correlation ◽  
Heteronuclear Correlation Spectroscopy ◽  
Angle Spinning

Interfaces Involving Biomolecules and Inorganic Materials: a Solid State NMR Approach

2007 ◽  
Vol 1008 ◽  
Author(s):  
Christian Bonhomme ◽  
Geoffrey Hartmeyer ◽  
Florence Babonneau ◽  
Michel Wong Chi Man ◽  
Guilhem Arrachart ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Chemical Nature ◽  
Sol Gel ◽  
Magic Angle Spinning ◽  
Inorganic Materials ◽  
Double Quantum ◽  
Magic Angle ◽  
Angle Spinning ◽  
Very High

AbstractMaterials based on ureidopyrimidinone (UPY) dimers and Adenine (A) / Thymine (T) derivatives were synthesized and characterized by advanced solid state NMR (Nuclear Magnetic Resonance) techniques. Silylated UPY molecules were used as model compounds, leading to structured organic-inorganic materials after hydrolysis and condensation processes (sol-gel reactions). High resolution 1H solid state NMR has been extensively used for the in-depth description of the H-bond networks, including very fast MAS (Magic Angle Spinning) experiments at very high field and DQ (double quantum) recoupling experiments. The chemical nature of the organic-inorganic interface has been illuminated by such techniques. In, particular, it has been demonstrated that H-bond networks were preserved during sol-gel reactions and were comparable to those observed in the UPY crystalline precursors.

Double-quantum filtering in magic-angle-spinning NMR spectroscopy applied to DNA oligomers

1996 ◽  
Vol 89 (6) ◽  
pp. 1835-1849 ◽  
Author(s):  
D.M. GREGORY ◽  
G.M. WOLFE ◽  
T.P. JARVIE ◽  
J.C. SHEILS ◽  
G.P. DROBNY
Keyword(s):  
Nmr Spectroscopy ◽  
Magic Angle Spinning ◽  
Double Quantum ◽  
Magic Angle ◽  
Dna Oligomers ◽  
Quantum Filtering ◽  
Angle Spinning

Deuterium double-quantum NMR with magic angle spinning

1980 ◽  
Vol 74 (2) ◽  
pp. 376-378 ◽  
Author(s):  
R. Eckman ◽  
L. Muller ◽  
A. Pines
Keyword(s):  
Magic Angle Spinning ◽  
Double Quantum ◽  
Magic Angle ◽  
Angle Spinning
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