scholarly journals Determination of Redox Reaction Rates and Orders by In Situ Liquid Cell Electron Microscopy of Pd and Au Solution Growth

2014 ◽  
Vol 136 (48) ◽  
pp. 16865-16870 ◽  
Author(s):  
Eli A. Sutter ◽  
Peter W. Sutter
Keyword(s):  
Electron Microscopy ◽  
Redox Reaction ◽  
Reaction Rates ◽  
Solution Growth ◽  
Liquid Cell

scholarly journals In-Situ Liquid Cell Electron Microscopy of the Solution Growth of Core-Shell Nanostructures

2014 ◽  
Vol 20 (S3) ◽  
pp. 1504-1505
Author(s):  
E. Sutter ◽  
K. Jungjohann ◽  
S. Bliznakov ◽  
E. A. Stach ◽  
A. Courty ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Solution Growth ◽  
Core Shell ◽  
Shell Nanostructures ◽  
Liquid Cell

In Situ Liquid Cell Electron Microscopy of the Solution Growth of Au–Pd Core–Shell Nanostructures

Nano Letters ◽  
2013 ◽  
Vol 13 (6) ◽  
pp. 2964-2970 ◽  
Author(s):  
K. L. Jungjohann ◽  
S. Bliznakov ◽  
P. W. Sutter ◽  
E. A. Stach ◽  
E. A. Sutter
Keyword(s):  
Electron Microscopy ◽  
Solution Growth ◽  
Core Shell ◽  
Shell Nanostructures ◽  
Liquid Cell

scholarly journals Dynamics of Nanoscale Dendrite Formation in Solution Growth Revealed Through in Situ Liquid Cell Electron Microscopy

Nano Letters ◽  
2018 ◽  
Vol 18 (10) ◽  
pp. 6427-6433 ◽  
Author(s):  
Matthew R. Hauwiller ◽  
Xiaowei Zhang ◽  
Wen-I Liang ◽  
Chung-Hua Chiu ◽  
Qian Zhang ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Solution Growth ◽  
Dendrite Formation ◽  
Liquid Cell

scholarly journals Fabrication of a liquid cell for in situ transmission electron microscopy

Microscopy ◽  
2020 ◽  
Author(s):  
Xiaoguang Li ◽  
Kazutaka Mitsuishi ◽  
Masaki Takeguchi
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Cost Effective ◽  
Production Method ◽  
Microscopy Imaging ◽  
Transmission Electron ◽  
In Situ Electron Microscopy ◽  
Liquid Cell ◽  
Si Wafer

Abstract Liquid cell transmission electron microscopy (LCTEM) enables imaging of dynamic processes in liquid with high spatial and temporal resolution. The widely used liquid cell (LC) consists of two stacking microchips with a thin wet sample sandwiched between them. The vertically overlapped electron-transparent membrane windows on the microchips provide passage for the electron beam. However, microchips with imprecise dimensions usually cause poor alignment of the windows and difficulty in acquiring high-quality images. In this study, we developed a new and efficient microchip fabrication process for LCTEM with a large viewing area (180 µm × 40 µm) and evaluated the resultant LC. The new positioning reference marks on the surface of the Si wafer dramatically improve the precision of dicing the wafer, making it possible to accurately align the windows on two stacking microchips. The precise alignment led to a liquid thickness of 125.6 nm close to the edge of the viewing area. The performance of our LC was demonstrated by in situ transmission electron microscopy imaging of the dynamic motions of 2-nm Pt particles. This versatile and cost-effective microchip production method can be used to fabricate other types of microchips for in situ electron microscopy.

In-situ liquid cell transmission electron microscopy guiding the design of large-sized cocatalysts coupled with ultra-small photocatalysts for highly efficient energy harvesting

2021 ◽  
Author(s):  
Chunlang Gao ◽  
Chunqiang Zhuang ◽  
Yuanli Li ◽  
Heyang Qi ◽  
Ge Chen ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Energy Harvesting ◽  
Design Strategy ◽  
Efficient Energy ◽  
Highly Efficient ◽  
Transmission Electron ◽  
Cell Transmission ◽  
Liquid Cell

In this study, we employed in-situ liquid cell transmission electron microscopy (LC-TEM) to carry out the new design strategy of precisely regulating the microstructure of large-sized cocatalysts for highly efficient...

In situ liquid cell electron microscopy of Ag–Au galvanic replacement reactions

Nanoscale ◽  
2017 ◽  
Vol 9 (3) ◽  
pp. 1271-1278 ◽  
Author(s):  
Eli A. Sutter ◽  
Peter W. Sutter
Keyword(s):  
Electron Microscopy ◽  
Galvanic Replacement ◽  
Liquid Cell
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