Specific 12CβD212CγD2S13CεHD2 Isotopomer Labeling of Methionine To Characterize Protein Dynamics by 1H and 13C NMR Relaxation Dispersion

Ulrich Weininger; Zhihong Liu; Deane D. McIntyre; Hans J. Vogel; Mikael Akke

doi:10.1021/ja309294u

Specific 12CβD212CγD2S13CεHD2 Isotopomer Labeling of Methionine To Characterize Protein Dynamics by 1H and 13C NMR Relaxation Dispersion

Journal of the American Chemical Society ◽

10.1021/ja309294u ◽

2012 ◽

Vol 134 (45) ◽

pp. 18562-18565 ◽

Cited By ~ 21

Author(s):

Ulrich Weininger ◽

Zhihong Liu ◽

Deane D. McIntyre ◽

Hans J. Vogel ◽

Mikael Akke

Keyword(s):

Protein Dynamics ◽

13C Nmr ◽

Nmr Relaxation ◽

Relaxation Dispersion ◽

1H And 13C Nmr

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Rotamer Jumps, Proton Exchange, and Amine Inversion Dynamics of Dimethylated Lysine Residues in Proteins Resolved by pH-Dependent 1H and 13C NMR Relaxation Dispersion

The Journal of Physical Chemistry B ◽

10.1021/acs.jpcb.9b06408 ◽

2019 ◽

Vol 123 (46) ◽

pp. 9742-9750

Author(s):

Ulrich Weininger ◽

Kristofer Modig ◽

Hiroaki Ishida ◽

Hans J. Vogel ◽

Mikael Akke

Keyword(s):

13C Nmr ◽

Nmr Relaxation ◽

Proton Exchange ◽

Relaxation Dispersion ◽

1H And 13C Nmr ◽

Lysine Residues ◽

Ph Dependent

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The conformation of cytochalasin D in DMSO solution from 1H and 13C NMR relaxation rates

Journal of the Chemical Society Perkin Transactions 2 ◽

10.1039/p29930000729 ◽

1993 ◽

pp. 729 ◽

Cited By ~ 2

Author(s):

Antonella Maccotta ◽

Gianni Valensin ◽

Nicola Gaggelli ◽

Elena Gaggelli

Keyword(s):

13C Nmr ◽

Nmr Relaxation ◽

Cytochalasin D ◽

Dmso Solution ◽

Relaxation Rates ◽

1H And 13C Nmr

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Structural and dynamical characterization of piroxicam by 1H- and 13C-NMR relaxation studies

Biophysical Chemistry ◽

10.1016/0301-4622(87)80065-0 ◽

1987 ◽

Vol 27 (3) ◽

pp. 255-261 ◽

Cited By ~ 5

Author(s):

Claudio Rossi ◽

Adriana Casini ◽

Maria Pia Picchi ◽

Franco Laschi ◽

Angela Calabria ◽

...

Keyword(s):

13C Nmr ◽

Nmr Relaxation ◽

1H And 13C Nmr ◽

Relaxation Studies

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1H and 13C NMR relaxation mechanisms of 1-methylimidazole bound to Cu(II) complexes.

Journal of Inorganic Biochemistry ◽

10.1016/0162-0134(91)84201-j ◽

1991 ◽

Vol 43 (2-3) ◽

pp. 209

Author(s):

M. Piccioli ◽

S. Ciurli

Keyword(s):

13C Nmr ◽

Nmr Relaxation ◽

1H And 13C Nmr

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1H and 13C NMR relaxation investigation of the copper(II) complex of amitraz, a formamidine pesticide

Polyhedron ◽

10.1016/s0277-5387(00)83053-3 ◽

1993 ◽

Vol 12 (19) ◽

pp. 2355-2358

Author(s):

Elena Gaggelli ◽

Nicola Gaggelli ◽

Gianni Valensin ◽

Alessandro Franchi

Keyword(s):

13C Nmr ◽

Nmr Relaxation ◽

1H And 13C Nmr

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Faculty Opinions recommendation of Dynamics of ligand binding from 13C NMR relaxation dispersion at natural abundance.

Faculty Opinions – Post-Publication Peer Review of the Biomedical Literature ◽

10.3410/f.1124154.581289 ◽

2008 ◽

Author(s):

H Jane Dyson ◽

Gira Bhabha

Keyword(s):

Ligand Binding ◽

13C Nmr ◽

Nmr Relaxation ◽

Natural Abundance ◽

Relaxation Dispersion

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Molecular mobility of counterion functional groups in ionic liquid 1-ethyl-3-methylimidazolium acetate according to 1H and 13C NMR relaxation data

Russian Chemical Bulletin ◽

10.1007/s11172-013-0288-6 ◽

2013 ◽

Vol 62 (9) ◽

pp. 1985-1990 ◽

Cited By ~ 7

Author(s):

V. V. Matveev ◽

D. A. Markelov ◽

V. I. Chizhik ◽

P. Ingman ◽

E. Lähderanta

Keyword(s):

Ionic Liquid ◽

Functional Groups ◽

13C Nmr ◽

Molecular Mobility ◽

Nmr Relaxation ◽

Relaxation Data ◽

1H And 13C Nmr

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The influence of pH on the coordination of copper(II) by 2-amino-2-deoxy-D-gluconate and 2-amino-2-deoxy-D-glucose oxime as studied by 1H and 13C NMR relaxation rate measurements and EPR spectroscopy

Inorganica Chimica Acta ◽

10.1016/s0020-1693(00)87347-8 ◽

1993 ◽

Vol 205 (1) ◽

pp. 1-7 ◽

Cited By ~ 13

Author(s):

Jacco van Haveren ◽

Herman van Bekkum ◽

Joop A. Peters

Keyword(s):

Relaxation Rate ◽

13C Nmr ◽

Epr Spectroscopy ◽

Nmr Relaxation ◽

1H And 13C Nmr ◽

Influence Of Ph

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1H and 13C NMR spectral assignments of the major sequences of twelve systematically modified heparin derivatives

Carbohydrate Research ◽

10.1016/s0008-6215(96)00213-3 ◽

1996 ◽

Vol 294 (1-4) ◽

pp. 15-27 ◽

Cited By ~ 40

Author(s):

E Yates

Keyword(s):

13C Nmr ◽

1H And 13C Nmr ◽

Heparin Derivatives

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Some Considerations Regarding the 1H and 13C Spectra of 4-(1-azulenyl)-2,6-bis(2-heteroaryl-vinyl)- pyrylium and Pyridinium and their Corresponding Pyridines

Revista de Chimie ◽

10.37358/rc.18.1.6045 ◽

2018 ◽

Vol 69 (1) ◽

pp. 64-69

Author(s):

Liviu Birzan ◽

Mihaela Cristea ◽

Constantin C. Draghici ◽

Alexandru C. Razus

Keyword(s):

Double Bond ◽

13C Nmr ◽

Nmr Spectra ◽

Chemical Shifts ◽

Pyridinium Salts ◽

13C Nmr Spectra ◽

1H And 13C Nmr ◽

Pyrylium Salts

The 1H and 13C NMR spectra of several 2,6-diheteroarylvinyl heterocycles containing 4-azulenyl moiety were recorded and their proton and carbon chemical shifts were compared with those of the compounds without double bond between the heterocycles. The influence of the nature of central and side heterocycles, molecule polarization and anisotropic effects were revealed. The highest chemical shifts were recorded for the pyrylium salts and the lowest at pyridines, but in the case of the pyridinium salts, the protons chemical shifts at the central heterocycle are more shielded due to a peculiar anisotropy of the attached vinyl groups.

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