Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO4

2012 ◽  
Vol 134 (43) ◽  
pp. 17889-17891 ◽  
Author(s):  
Kang Min Ok ◽  
Dong Woo Lee ◽  
Ronald I. Smith ◽  
Dermot O’Hare
Keyword(s):  
Neutron Diffraction ◽  
Hydrothermal Conditions ◽  
Time Resolved ◽  
In Situ Neutron Diffraction

scholarly journals Time-Resolved In Situ Neutron Diffraction Study of Cu22Fe8Ge4S32 Germanite: A Guide for the Synthesis of Complex Chalcogenides

2020 ◽  
Vol 32 (20) ◽  
pp. 8993-9000
Author(s):  
Laura Paradis-Fortin ◽  
Pierric Lemoine ◽  
Carmelo Prestipino ◽  
Ventrapati Pavan Kumar ◽  
Bernard Raveau ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Diffraction Study ◽  
Neutron Diffraction Study ◽  
Time Resolved ◽  
In Situ Neutron Diffraction

scholarly journals Time-resolved in situ neutron diffraction studies of Li-ion battery materials

2014 ◽  
Vol 70 (a1) ◽  
pp. C353-C353 ◽  
Author(s):  
Neeraj Sharma
Keyword(s):  
Crystal Structure ◽  
Neutron Diffraction ◽  
Lithium Ion Batteries ◽  
Lithium Ion ◽  
Electrochemical Process ◽  
Atomic Scale ◽  
Structure Evolution ◽  
Time Resolved ◽  
In Situ Neutron Diffraction

Lithium-ion batteries are ubiquitous in society, used in everything from children's toys to mobile electronic devices, providing portable power solutions. There is a continuous drive for the improvement of these batteries to meet the demands of higher power devices and uses. A large proportion of the function of lithium-ion batteries arises from the electrodes, and these are in turn mediated by the atomic-scale perturbations or changes in the crystal structure during an electrochemical process (e.g. battery use). Therefore, a method to both understand battery function and propose ideas to improve their performance is to probe the electrode crystal structure evolution in situ while an electrochemical process is occurring inside a battery. Our work has utilized the benefits of in situ neutron diffraction (e.g. sensitivity towards lithium) to literally track the time-resolved evolution of lithium in electrode materials used in lithium-ion batteries (see Figure 1). With this knowledge we have been able to directly relate electrochemical properties such as capacity and differences in charge/discharge behaviour of a battery to the content and distribution of lithium in the electrode crystal structure. This talk will showcase some of our in situ investigations of materials in lithium-ion batteries, such as LiCoO2, LiFePO4, Li1+yMn2O4, LiNi0.5Mn1.5O4 and Li4Ti5O12/TiO2 electrodes. In addition, selected examples of our work using time-resolved in situ X-ray diffraction to probe other batteries types, such as primary lithium and secondary (rechargeable) sodium-ion batteries will be presented. Using time-resolved diffraction data, a comprehensive atomic-scale picture of battery functionality can be modelled and permutations can be made to the electrodes and electrochemical conditions to optimize battery performance. Therefore, crystallography and electrochemistry can mesh together to solve our energy needs.

Time-Resolved in Situ Neutron Diffraction Studies of Gas Hydrate:  Transformation of Structure II (sII) to Structure I (sI)

2001 ◽  
Vol 123 (51) ◽  
pp. 12826-12831 ◽  
Author(s):  
Yuval Halpern ◽  
Vu Thieu ◽  
Robert W. Henning ◽  
Xiaoping Wang ◽  
Arthur J. Schultz
Keyword(s):  
Neutron Diffraction ◽  
Gas Hydrate ◽  
Time Resolved ◽  
In Situ Neutron Diffraction

Study of tempering behavior of lath martensite using in situ neutron diffraction

2015 ◽  
Vol 107 ◽  
pp. 29-32 ◽  
Author(s):  
Z.M. Shi ◽  
W. Gong ◽  
Y. Tomota ◽  
S. Harjo ◽  
J. Li ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Lath Martensite ◽  
In Situ Neutron Diffraction

In situ neutron diffraction study of fatigue behavior of CrFeCoNiMo0.2 high entropy alloy

2021 ◽  
Vol 139 ◽  
pp. 107371
Author(s):  
Haiyan He ◽  
Bing Wang ◽  
Dong Ma ◽  
Alexandru D. Stoica ◽  
Zhenduo Wu ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Diffraction Study ◽  
Fatigue Behavior ◽  
Neutron Diffraction Study ◽  
High Entropy Alloy ◽  
High Entropy ◽  
In Situ Neutron Diffraction
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