Transformation of a Close-Packed Au Nanoparticle/Polymer Monolayer into a Large Area Array of Oriented Au Nanowires via E-beam Promoted Uniaxial Deformation and Room Temperature Sintering

2011 ◽  
Vol 133 (30) ◽  
pp. 11410-11413 ◽  
Author(s):  
Shisheng Xiong ◽  
Ryan Molecke ◽  
Matthew Bosch ◽  
P. Randall Schunk ◽  
C. Jeffrey Brinker
Author(s):  
D. L. Rohr ◽  
S. S. Hecker

As part of a comprehensive study of microstructural and mechanical response of metals to uniaxial and biaxial deformations, the development of substructure in 1100 A1 has been studied over a range of plastic strain for two stress states.Specimens of 1100 aluminum annealed at 350 C were tested in uniaxial (UT) and balanced biaxial tension (BBT) at room temperature to different strain levels. The biaxial specimens were produced by the in-plane punch stretching technique. Areas of known strain levels were prepared for TEM by lapping followed by jet electropolishing. All specimens were examined in a JEOL 200B run at 150 and 200 kV within 24 to 36 hours after testing.The development of the substructure with deformation is shown in Fig. 1 for both stress states. Initial deformation produces dislocation tangles, which form cell walls by 10% uniaxial deformation, and start to recover to form subgrains by 25%. The results of several hundred measurements of cell/subgrain sizes by a linear intercept technique are presented in Table I.


2003 ◽  
Vol 775 ◽  
Author(s):  
Jeffrey Anderson ◽  
Rubi Garcia ◽  
Weilie L. Zhou

AbstractSubmicron KMnF3 cubic and spherical nanoparticles were synthesized using the reverse micelle method. The nanostructures of the nanocrystals were studied by field emission electron microscopy and transmission electron microscopy. KMnF3 nanocrystals synthesized at room temperature started with cubic submicron particles (∼100 nm) and consisted of KMnF3 nanocrystallites (10-15 nm). As the reaction continued, the nanocrystals fused together and transformed into perfect cubic nanocrystals. Spherical beads composed of KMnF3 nanocrystallites were observed at low temperature synthesis. As the reaction continued, the spherical particles grew larger, however, no characteristic cubic shape of KMnF3 nanoparticles were observed. Even as they grew larger, there was no evidence of homogeneous crystal morphology as seen in the room temperature samples. Cubic shape KMnF3 nanocrystals were self-assembled into large area self-assembling patterns.


2016 ◽  
Vol 24 (23) ◽  
pp. 26097 ◽  
Author(s):  
Zhen Li ◽  
Shouzhen Jiang ◽  
Yanyan Huo ◽  
Mei Liu ◽  
Cheng Yang ◽  
...  
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