AN ANHYDROUS DISTILLATION METHOD FOR THE DETERMINATION OF CERTAIN METALS IN ORGANIC COMPOUNDS. I. THE DETERMINATION OF MERCURY

1931 ◽  
Vol 53 (7) ◽  
pp. 2468-2475 ◽  
Author(s):  
E. P. Fenimore ◽  
E. C. Wagner
Keyword(s):  
Organic Compounds ◽  
Distillation Method

An Automated Procedure for the Determination of Ammonia in Tobacco

1972 ◽  
Vol 6 (4) ◽  
Author(s):  
P.F. Collins ◽  
W.W. Lawrence ◽  
J.F. Williams
Keyword(s):  
Standard Deviation ◽  
Relative Standard Deviation ◽  
Distillation Method ◽  
Relative Standard ◽  
Tobacco Sample ◽  
Automated Determination

AbstractA procedure for the automated determination of ammonia in tobacco has been developed. Ammonia is extracted from the ground tobacco sample with water and is determined with a Technicon Auto Analyser system which employs separation of the ammonia through volatilization followed by colourimetry using the phenate-hypochlorite reaction. The procedure has been applied to a variety of tobaccos containing from 0.02 to 0.5 % ammonia with an overall relative standard deviation of 2 %. The accuracy of the procedure as judged by recovery tests and by comparison to a manual distillation method is considered adequate

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