Surfaces of Solids. XIII. A Vapor Adsorption Method for the Determination of the Area of a Solid without the Assumption of a Molecular Area, and the Areas Occupied by Nitrogen and Other Molecules on the Surface of a Solid

1944 ◽  
Vol 66 (8) ◽  
pp. 1366-1373 ◽  
Author(s):  
William D. Harkins ◽  
George Jura
Keyword(s):  
Molecular Area ◽  
Adsorption Method ◽  
Vapor Adsorption

APPLICATION OF ADSORPTION METHOD FOR DETERMINATION OF LOCAL CONVECTIVE HEAT TRANSFER RATES

1974 ◽  
Author(s):  
S. Koncar-Djurdjevic ◽  
M. Mitrovic ◽  
S. Cvijovic ◽  
G. Popovic ◽  
Dimitrije Voronjec
Keyword(s):  
Heat Transfer ◽  
Convective Heat Transfer ◽  
Convective Heat ◽  
Adsorption Method ◽  
Transfer Rates

scholarly journals Immobilization of Isolated Lipase From Moldy Copra(Aspergillus Oryzae)

2011 ◽  
Vol 8 (2) ◽  
pp. 896-902
Author(s):  
Seniwati Dali ◽  
A. B. D. Rauf Patong ◽  
M. Noor Jalaluddin ◽  
Pirman ◽  
Baharuddin Hamzah
Keyword(s):  
Thermal Stability ◽  
Aspergillus Oryzae ◽  
Immobilized Lipase ◽  
Optimum Temperature ◽  
Adsorption Method ◽  
Ph Optimum ◽  
Optimum Ph ◽  
Recovery Technique ◽  
Free Lipase

Enzyme immobilization is a recovery technique that has been studied in several years, using support as a media to help enzyme dissolutions to the reaction substrate. Immobilization method used in this study was adsorption method, using specific lipase fromAspergillus oryzae. Lipase was partially purified from the culture supernatant ofAspergillus oryzae. Enzyme was immobilized by adsorbed on silica gel. Studies on free and immobilized lipase systems for determination of optimum pH, optimum temperature, thermal stability and reusability were carried out. The results showed that free lipase had optimum pH 8,2 and optimum temperature 35 °C while the immobilized lipase had optimum 8,2 and optimum temperature 45 °C. The thermal stability of the immobilized lipase, relative to that of the free lipase, was markedly increased. The immobilized lipase can be reused for at least six times.

Dye adsorption revisited: Application of the cationic dye adsorption method for the quantitative determination of the acidic surface groups of nanocellulose materials

2021 ◽  
Author(s):  
Jun Araki
Keyword(s):  
Dye Adsorption ◽  
Carboxyl Groups ◽  
Cationic Dye ◽  
Cellulose Nanowhiskers ◽  
Adsorption Method ◽  
Short Period ◽  
Light Absorbance ◽  
Mercapto Groups ◽  
Rapid Treatment

Abstract The surface carboxyl and sulfate groups on cellulose nanowhiskers were quantified via the adsorption of toluidine blue O (TBO), a cationic dye. Here, simple and rapid protocols, such as mixing the nanowhisker suspensions with a dye solution, separating the supernatants via centrifugation, and determining the excess dye concentration via visible light absorbance techniques, were used to obtain reproducible results comparable with those obtained via titration. In addition to facilitating the discrete quantification of the sulfate and carboxyl groups, the TBO adsorption method enabled carboxyl quantification in the presence of mercapto groups, which was difficult to achieve via titration. The adsorption of TBO onto the carboxyl groups was completed within 30 min, enabling the rapid treatment of many samples within a short period.

scholarly journals Determination of porous structure parameters of coal particles to describe thermal conversion processes

2019 ◽  
Vol 109 ◽  
pp. 00101
Author(s):  
Oleksandr Topal ◽  
Iryna Holenko ◽  
Inna Diakun
Keyword(s):  
Porous Structure ◽  
Gas Adsorption ◽  
Thermal Conversion ◽  
Structure Parameters ◽  
Adsorption Method ◽  
Coal Particles ◽  
Different Temperatures ◽  
Char Reactivity ◽  
Determination Of Parameters

The results of determination of parameters of porous structure of coal and char particles are presented. They were determined using gas adsorption method and thermal decomposition of particles in air oxygen. The porous structure parameters allow predicting char reactivity change at different temperatures as well as during conversion in accordance with Random Pore Model (RPM-model).

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