Crystal structure of a versatile organic clathrate. 4-p-Hydroxyphenyl-2,2,4-trimethylchroman (Dianin's compound)

1970 ◽  
Vol 92 (12) ◽  
pp. 3749-3755 ◽  
Author(s):  
J. L. Flippen ◽  
Jerome. Karle ◽  
Isabella L. Karle
Keyword(s):  
Crystal Structure ◽  
Dianin's Compound

The crystal structure and thermal expansion of the CCl4 adduct of Dianin's compound

1990 ◽  
Vol 68 (8) ◽  
pp. 1352-1356 ◽  
Author(s):  
Walter Abriel ◽  
André Du Bois ◽  
Marek Zakrzewski ◽  
Mary Anne White
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Guest Molecules ◽  
X Ray ◽  
Thermal Expansion Coefficients ◽  
Expansion Coefficients ◽  
Dianin's Compound

The crystal structure of the title compound has been determined by single crystal X-ray diffraction data collected at 293 K, and refined to a final Rw of 0.057. The crystals are rhombohedral, space group [Formula: see text], with a = 27.134(8) Å, c = 10.933(2) Å, and Z = 18. The mole ratio of Dianin's compound (4-p-hydroxyphenyl-2,2,4-trimethylchroman) to CCl4 is 6:1. The guest molecules are disordered. X-ray powder diffraction was carried out in the temperature range from 10 to 300 K. From this, the thermal expansion coefficients for the a- and c-axes and the volume have been determined. Keywords: thermal expansion, crystal structure, clathrate.

Crystal structure of a clathrate formed by a mercapto-analogue of Dianin's compound

1977 ◽  
pp. 292 ◽  
Author(s):  
Andrew D. U. Hardy ◽  
David D. MacNicol ◽  
Joseph J. McKendrick ◽  
Derek R. Wilson
Keyword(s):  
Crystal Structure ◽  
Dianin's Compound

Crystal structure and13C CP/MAS NMR of thep-xylene clathrate of Dianin's compound

1999 ◽  
Vol 97 (11) ◽  
pp. 1193-1196 ◽  
Author(s):  
G. D. ENRIGHT ◽  
C. I. RATCLIFFE ◽  
J. A. RIPMEESTER
Keyword(s):  
Crystal Structure ◽  
Mas Nmr ◽  
Cp Mas Nmr ◽  
Dianin's Compound

Crystal structure and 13C CP/MAS NMR of the p-xylene clathrate of Dianin's compound

1999 ◽  
Vol 97 (11) ◽  
pp. 1193-1196 ◽  
Author(s):  
G. D. Enright, C. I. Ratcliffe, J. A.
Keyword(s):  
Crystal Structure ◽  
Mas Nmr ◽  
Cp Mas Nmr ◽  
Dianin's Compound ◽  
13C Cp Mas Nmr

Crystal structure, CP/MAS xeon-129 and carbon-13 NMR of local ordering in Dianin's compound clathrates

1988 ◽  
Vol 110 (18) ◽  
pp. 6014-6019 ◽  
Author(s):  
F. Lee ◽  
E. Gabe ◽  
J. S. Tse ◽  
J. A. Ripmeester
Keyword(s):  
Crystal Structure ◽  
Local Ordering ◽  
Dianin's Compound

Temperature-dependent crystal structure of the isopropanol clathrate of Dianin's compound

2011 ◽  
Vol 47 (7) ◽  
pp. 2029 ◽  
Author(s):  
Jackson J. Lee ◽  
Rebecca O. Fuller ◽  
Alexandre N. Sobolev ◽  
Henrik F. Clausen ◽  
Jacob Overgaard ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Temperature Dependent ◽  
Dianin's Compound
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