Dipolar NMR spectroscopy of nonoxidic glasses. Structural characterization of the system phosphorus-selenium by phosphorus-31-selenium-77 spin echo double resonance NMR

1990 ◽  
Vol 112 (24) ◽  
pp. 9017-9019 ◽  
Author(s):  
D. Lathrop ◽  
H. Eckert
Keyword(s):  
Nmr Spectroscopy ◽  
Structural Characterization ◽  
Spin Echo ◽  
Double Resonance

scholarly journals Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1207
Author(s):  
Gabrielle Foran ◽  
Nina Verdier ◽  
David Lepage ◽  
Cédric Malveau ◽  
Nicolas Dupré ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Pulse Sequence ◽  
Dynamic Properties ◽  
Double Resonance ◽  
Solid Polymer ◽  
Pulse Field ◽  
Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

11B{15N} REDOR and11B Spin Echo Studies for structural characterization of Si‐B‐C‐N precursor ceramics

2007 ◽  
Vol 4 (2-4) ◽  
pp. 207-225 ◽  
Author(s):  
Thomas Emmler ◽  
Otgontuul Tsetsgee ◽  
Gerd Buntkowsky ◽  
Markus Weinmann ◽  
Fritz Aldinger ◽  
...  
Keyword(s):  
Structural Characterization ◽  
Spin Echo

Structural characterization of ionomer glasses by multinuclear solid state MAS-NMR spectroscopy

2007 ◽  
Vol 353 (3) ◽  
pp. 237-243 ◽  
Author(s):  
Shigeki Matsuya ◽  
Artemis Stamboulis ◽  
Robert G. Hill ◽  
Robert V. Law
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Structural Characterization ◽  
Mas Nmr
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