A mixed aggregate of lithium diisopropylamide and lithium chloride: synthesis and crystal structure

1993 ◽  
Vol 115 (8) ◽  
pp. 3388-3389 ◽  
Author(s):  
Francis S. Mair ◽  
William Clegg ◽  
Paul A. O'Neil
1991 ◽  
Vol 46 (2) ◽  
pp. 143-146 ◽  
Author(s):  
F. Ekkehardt Hahn ◽  
Stefan Rupprecht

The reaction of lithiated catechol ligands with W (0)Cl4 produces LiCl as a side product. The lithium chloride from this reaction crystallizes as (THF)2Li(μ-Cl)-,Li(THF)2. The X -ray analysis shows lithium in the center of a distorted tetrahedron made up from two THF molecules and two bridging chlorides with d(Li-Cl) = 2.342(3) and 2.308(3)Å.


2002 ◽  
Vol 2002 (3) ◽  
pp. 120-121
Author(s):  
Tian Fu Liu ◽  
Hua Kuan Lin ◽  
Shou Rong Zhu ◽  
Zhong Ming Wang ◽  
Hong Gen Wang ◽  
...  

2002 ◽  
Vol 2002 (3) ◽  
pp. 107-109 ◽  
Author(s):  
Guang Liu ◽  
Jian Liu ◽  
Shi-Wei Zhang

1992 ◽  
Author(s):  
W. T. Harrison ◽  
G. D. Stucky ◽  
R. E. Morris ◽  
A. K. Cheetham

2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.


2019 ◽  
Vol 35 (0) ◽  
pp. 27-29
Author(s):  
Reiko YAGUCHI ◽  
Hideki FURUTACHI ◽  
Sanae SHIROTSUKI ◽  
Xi ZHANG ◽  
Takanao ISHIKAWA ◽  
...  

Author(s):  
Mohammad Usman ◽  
Gyanendra B. Ayer ◽  
Mark D. Smith ◽  
Hans-Conrad zur Loye

1992 ◽  
Vol 195 (3-4) ◽  
pp. 335-344 ◽  
Author(s):  
C. Chaillout ◽  
Q. Huang ◽  
R.J. Cava ◽  
J. Chenavas ◽  
A. Santoro ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document