An x-ray crystallographic and high-field NMR study of chromium complexes [(C6Et6)Cr(CO)2NO]+BF4- and [(C6Et6)Cr(CO)(CS)NO]+BF4-: steric inhibition of tripodal rotation

1991 ◽  
Vol 113 (4) ◽  
pp. 1177-1185 ◽  
Author(s):  
Bavani Mailvaganam ◽  
Christopher S. Frampton ◽  
Siden Top ◽  
Brian G. Sayer ◽  
Michael J. McGlinchey
Keyword(s):  
High Field ◽  
Chromium Complexes ◽  
X Ray ◽  
Nmr Study

High-field NMR study of vertex rotation in (C5HnMe5-n)MCo2(CO)8CR clusters (M = molybdenum, tungsten): x-ray crystal structure of (C5Me5)MoCo2(CO)8CCO2-iso-Pr

1991 ◽  
Vol 10 (7) ◽  
pp. 2362-2370 ◽  
Author(s):  
Karen A. Sutin ◽  
Lijuan. Li ◽  
Christopher S. Frampton ◽  
Brian G. Sayer ◽  
Michael J. McGlinchey
Keyword(s):  
Crystal Structure ◽  
High Field ◽  
X Ray ◽  
Nmr Study

Stereochemical Study of a Bradicardisant Benzazepine-Type Drug. X-Ray Structure of the Chloride Salt and High-Field NMR Study of the Stereochemistry in Solution

1997 ◽  
Vol 35 (3) ◽  
pp. 175-183 ◽  
Author(s):  
Delphine Duval ◽  
Philippe Hennig ◽  
Jean Paul Bouchet ◽  
Joel Vian ◽  
Jean Louis Peglion ◽  
...  
Keyword(s):  
High Field ◽  
Chloride Salt ◽  
X Ray ◽  
Nmr Study

Crystal and solution structure of (E)-1,2-bis(ethylsulphonyl)cyclobutane-1,2-dicarbonitrile

1989 ◽  
Vol 54 (12) ◽  
pp. 3253-3259
Author(s):  
Jaroslav Podlaha ◽  
Miloš Buděšínský ◽  
Jana Podlahová ◽  
Jindřich Hašek
Keyword(s):  
Hydrogen Peroxide ◽  
Solution Structure ◽  
Peroxide Oxidation ◽  
X Ray ◽  
X Ray Crystallography ◽  
Nmr Study ◽  
Hydrogen Peroxide Oxidation ◽  
Unusual Product ◽  
C Nmr

The unusual product of the reaction of 2-chloroacrylonitrile with ethane thiol and following hydrogen peroxide oxidation was found to be (E)-1,2-bis(ethylsulphonyl)cyclobutane-1,2-dicarbonitrile by means of X-ray crystallography. 1H and 13C NMR study of this compound has proven the same conformation of the molecule in solution.

High-field soft-x-ray dichroism of a hard ferrimagnet with easy-plane anisotropy

2021 ◽  
Vol 104 (6) ◽  
Author(s):  
Sh. Yamamoto ◽  
D. I. Gorbunov ◽  
I. F. Diaz-Ortega ◽  
A. Miyata ◽  
T. Kihara ◽  
...  
Keyword(s):  
High Field ◽  
Easy Plane ◽  
X Ray ◽  
Plane Anisotropy

scholarly journals Tautomerisation in 1-(4-Methylphenylazo)naphthalen-2-ol and 2-(4-Methylphenylazo)-4-methylphenol: A Crystallographic and 13C{1H}NMR Study

1999 ◽  
Vol 23 (3) ◽  
pp. 178-179
Author(s):  
Wendy I. Cross ◽  
Kevin R. Flower ◽  
Robin G. Pritchard
Keyword(s):  
Acetic Acid ◽  
Nmr Spectroscopy ◽  
Resonant Frequency ◽  
X Ray Diffraction ◽  
X Ray ◽  
H Nmr ◽  
Nmr Study ◽  
Acetic Acid Esters ◽  
Acid Esters ◽  
Equivalent Carbon

The acetic acid esters of 1-(4-methylphenylazo)naphthalen-2-ol 1 and 2-(4-methylphenylazo)-4-methylphenol 3 are prepared and characterised by single crystal X-ray diffraction studies and 13C{1H}NMR spectroscopy; the position of the C(2)13C resonance for the ester is used to predict the position of resonant frequency of the equivalent carbon in the parent alcohols and hence, calculate the position of the azo-hydrazone equilibrium in these compounds.

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