Chemical Processing in high-pressure aqueous environments. 3. Batch reactor process development experiments for organics destruction

1994 ◽  
Vol 33 (3) ◽  
pp. 558-565 ◽  
Author(s):  
Douglas C. Elliott ◽  
L. John Jr. Sealock ◽  
Eddie G. Baker
Keyword(s):  
High Pressure ◽  
Process Development ◽  
Batch Reactor ◽  
Chemical Processing ◽  
Aqueous Environments

Chemical Processing in High-Pressure Aqueous Environments. 9. Process Development for Catalytic Gasification of Algae Feedstocks

2012 ◽  
Vol 51 (33) ◽  
pp. 10768-10777 ◽  
Author(s):  
Douglas C. Elliott ◽  
Todd R. Hart ◽  
Gary G. Neuenschwander ◽  
Leslie J. Rotness ◽  
Mariefel V. Olarte ◽  
...  
Keyword(s):  
High Pressure ◽  
Process Development ◽  
Chemical Processing ◽  
Catalytic Gasification ◽  
Aqueous Environments

Chemical Processing in High-Pressure Aqueous Environments. 7. Process Development for Catalytic Gasification of Wet Biomass Feedstocks

2004 ◽  
Vol 43 (9) ◽  
pp. 1999-2004 ◽  
Author(s):  
Douglas C. Elliott ◽  
Gary G. Neuenschwander ◽  
Todd R. Hart ◽  
R. Scott Butner ◽  
Alan H. Zacher ◽  
...  
Keyword(s):  
High Pressure ◽  
Process Development ◽  
Chemical Processing ◽  
Catalytic Gasification ◽  
Biomass Feedstocks ◽  
Wet Biomass ◽  
Aqueous Environments

Chemical Processing in High-Pressure Aqueous Environments. 5. New Processing Concepts

1996 ◽  
Vol 35 (11) ◽  
pp. 4111-4118 ◽  
Author(s):  
L. John Sealock ◽  
Douglas C. Elliott ◽  
Eddie G. Baker ◽  
Alexander G. Fassbender ◽  
Laura J. Silva
Keyword(s):  
High Pressure ◽  
Chemical Processing ◽  
Aqueous Environments ◽  
New Processing

Chemical processing in high-pressure aqueous environments. 1. Historical perspective and continuing developments

1993 ◽  
Vol 32 (8) ◽  
pp. 1535-1541 ◽  
Author(s):  
L. John Sealock ◽  
Douglas C. Elliott ◽  
Eddie G. Baker ◽  
R. Scott Butner
Keyword(s):  
High Pressure ◽  
Historical Perspective ◽  
Chemical Processing ◽  
Aqueous Environments

Intensification of the Production of 2-Ethyl-Hexyl Acrylate: Batch Kinetics and Reactive Distillation

2018 ◽  
Vol 16 (7) ◽  
Author(s):  
Vivek D. Talnikar ◽  
Onkar A. Deorukhkar ◽  
Amit Katariya ◽  
Yogesh S. Mahajan
Keyword(s):  
Kinetic Model ◽  
Acrylic Acid ◽  
Process Development ◽  
Reactive Distillation ◽  
Batch Reactor ◽  
Process Intensification ◽  
Complete Conversion ◽  
Reaction Conditions ◽  
Batch Mode ◽  
Batch Kinetics

Abstract The reaction of acrylic acid and 2-ethyl-1 hexanol was explored in this work with the intent of process intensification. In order to assess the effect of important parameters on the course of reaction, this work initially conducted batch reactor experiments. Reaction conditions in the batch reactor for a specific conversion (~ 30 %) were obtained. A kinetic model was then obtained through regression to arrive at a rate expression that is later used in process development. Experiments were performed in the reactive distillation (RD) environment in batch mode, which showed substantial increase in conversion (~ 80 %) indicating the applicability of RD. Further, this work performed simulation in the RD environment to assess process intensification. Simulations show that it is possible to obtain complete conversion of the acid.

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