Preparation, solution dynamics and x-ray crystal structure of the anilide-bridged diruthenium complex [(.eta.6-C6Me6)2Ru2(.mu.-NHPh)3][BF4]

1990 ◽  
Vol 29 (10) ◽  
pp. 2027-2030 ◽  
Author(s):  
Gaines C. Martin ◽  
Gus J. Palenik ◽  
James M. Boncella
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Diruthenium Complex

X-ray crystal structure and hydrocarbon solution dynamics of tetrameric 1-(dimethylamino)-3-lithiopropane

1985 ◽  
Vol 107 (26) ◽  
pp. 8292-8294 ◽  
Author(s):  
Gerhard W. Klumpp ◽  
Marcel Vos ◽  
Franciscus J. J. De Kanter ◽  
Cees Slob ◽  
Hendrik Krabbendam ◽  
...  
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Hydrocarbon Solution

X-ray crystal structure and hydrocarbon solution dynamics of dimeric 1,1-bis[(dimethylamino)methyl]-2-propyllithium

1989 ◽  
Vol 111 (9) ◽  
pp. 3463-3465 ◽  
Author(s):  
Willem Moene ◽  
Marcel Vos ◽  
Franciscus J. J. De Kanter ◽  
Gerhard W. Klumpp ◽  
Anthony L. Spek
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Hydrocarbon Solution

ChemInform Abstract: X-Ray Crystal Structure and Hydrocarbon Solution Dynamics of Tetrameric 1-(Dimethylamino)-3-lithiopropane

1986 ◽  
Vol 17 (16) ◽  
Author(s):  
G. W. KLUMPP ◽  
M. VOS ◽  
F. J. J. DE KANTER ◽  
C. SLOB ◽  
H. KRABBENDAM ◽  
...  
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Hydrocarbon Solution

ChemInform Abstract: X-Ray Crystal Structure and Hydrocarbon Solution Dynamics of Dimeric 1,1-Bis((dimethylamino)methyl)-2-propyllithium.

ChemInform ◽  
1989 ◽  
Vol 20 (32) ◽  
Author(s):  
W. MOENE ◽  
M. VOS ◽  
F. J. J. DE KANTER ◽  
G. W. KLUMPP ◽  
A. L. SPEK
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Hydrocarbon Solution

Dehydrogenation of Formic Acid Catalyzed by Water-Soluble Ruthenium Complexes: X-ray Crystal Structure of a Diruthenium Complex

2019 ◽  
Vol 2019 (7) ◽  
pp. 1046-1053 ◽  
Author(s):  
Soumyadip Patra ◽  
Mahendra K. Awasthi ◽  
Rohit K. Rai ◽  
Hemanta Deka ◽  
Shaikh M. Mobin ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Formic Acid ◽  
Ruthenium Complexes ◽  
Water Soluble ◽  
X Ray ◽  
Acid Catalyzed ◽  
Diruthenium Complex

Synthesis and crystal structure of a homoleptic diruthenium complex containing tetra-2-pyridyl-1,4-pyrazine (tppz)

2017 ◽  
Vol 72 (10) ◽  
pp. 759-762 ◽  
Author(s):  
Marion Graf ◽  
Peter Mayer ◽  
Hans-Christian Böttcher
Keyword(s):  
Molecular Structure ◽  
Crystal Structure ◽  
Mass Spectrometry ◽  
Nmr Spectroscopy ◽  
Title Complex ◽  
Dinuclear Complex ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
X Ray Crystallography ◽  
Diruthenium Complex

AbstractTreatment of hydrated ruthenium(III) chloride with tetra-2-pyridyl-1,4-pyrazine (tppz) in refluxing ethoxyethanol afforded the homoleptic dinuclear complex [(tppz)Ru(μ-tppz)Ru(tppz)]4+ (1) besides small amounts of the species [Ru(tppz)2]2+. The title complex 1 was obtained as purple crystals and characterized as its hexafluoridophosphate salt by NMR spectroscopy, mass spectrometry and microanalyses. The molecular structure of 1(PF6)4 has been established by X-ray crystallography.

Synthesis, Solution Dynamics, and X-ray Crystal Structure of Bis(2,4,6-tris(trifluoromethyl)- phenyl)(1,2-dimethoxyethane)nickel

2001 ◽  
Vol 20 (12) ◽  
pp. 2565-2569 ◽  
Author(s):  
George M. Benedikt ◽  
Brian L. Goodall ◽  
Suri Iyer ◽  
Lester H. McIntosh ◽  
Richard Mimna ◽  
...  
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Solution Dynamics ◽  
Synthesis Solution

A study on α-RuCl3 crystal structure by scanning tunneling microscopy

1989 ◽  
Vol 47 ◽  
pp. 30-31
Author(s):  
H.-J. Cantow ◽  
H. Hillebrecht ◽  
S. Magonov ◽  
H. W. Rotter ◽  
G. Thiele
Keyword(s):  
Crystal Structure ◽  
Density Distribution ◽  
Scanning Tunneling Microscopy ◽  
Electron Density ◽  
Structure Determination ◽  
Electron Density Distribution ◽  
Scanning Tunneling ◽  
Monoclinic Space Group ◽  
Tunneling Microscopy ◽  
X Ray

From X-ray analysis, the conclusions are drawn from averaged molecular informations. Thus, limitations are caused when analyzing systems whose symmetry is reduced due to interatomic interactions. In contrast, scanning tunneling microscopy (STM) directly images atomic scale surface electron density distribution, with a resolution up to fractions of Angstrom units. The crucial point is the correlation between the electron density distribution and the localization of individual atoms, which is reasonable in many cases. Thus, the use of STM images for crystal structure determination may be permitted. We tried to apply RuCl3 - a layered material with semiconductive properties - for such STM studies. From the X-ray analysis it has been assumed that α-form of this compound crystallizes in the monoclinic space group C2/m (AICI3 type). The chlorine atoms form an almost undistorted cubic closed package while Ru occupies 2/3 of the octahedral holes in every second layer building up a plane hexagon net (graphite net). Idealizing the arrangement of the chlorines a hexagonal symmetry would be expected. X-ray structure determination of isotypic compounds e.g. IrBr3 leads only to averaged positions of the metal atoms as there exist extended stacking faults of the metal layers.

X-ray Crystal Structure of ?9-THC-tosylate

Planta Medica ◽  
2008 ◽  
Vol 74 (03) ◽  
Author(s):  
W Gul ◽  
P Carvalho ◽  
D Slade ◽  
M Avery ◽  
JR Duchek ◽  
...  
Keyword(s):  
Crystal Structure ◽  
X Ray
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