Determination of Free Gossypol in Cottonseed Meal. A Colorimetric Method

1943 ◽  
Vol 15 (8) ◽  
pp. 489-491 ◽  
Author(s):  
Carl Lyman ◽  
Bryant Holland ◽  
Fred Hale
Keyword(s):  
Cottonseed Meal ◽  
Free Gossypol ◽  
Colorimetric Method

The Need for Using An Enzymatic Colorimetric Assay in Creatinine Determination of Peritoneal Dialysis Solutions

1990 ◽  
Vol 10 (1) ◽  
pp. 89-92 ◽  
Author(s):  
Liliane Larpent ◽  
Christian Verger
Keyword(s):  
Peritoneal Dialysis ◽  
Reliable Method ◽  
Colorimetric Assay ◽  
Colorimetric Method ◽  
Peritoneal Membrane ◽  
Creatinine Kinetics ◽  
Dialysis Solutions ◽  
Peritoneal Dialysis Solutions ◽  
Enzymatic Test

The fate of the peritoneal membrane on continuous ambulatory peritoneal dialysis (CAPD) is usually evaluated through the modification of its permeability to various solutes as glucose, creatinine, and urea. Therefore, the accuracy of the methods used for measurements of creatinine is of great importance. A particular problem does exist for creatinine determination as it may be influenced by the presence of glucose. We studied a new enzymatic colorimetric method for creatinine determination in peritoneal dialysis solutions which contain high dextrose concentrations. Creatinine was measured in plasma, urine, and dialysate from 18 patients on CAPD and in pure dextrose solutions, with an enzymatic test (Boehringer Mannheim) and with Jaffe's reaction on two different analyzers: Astra (Beckman) and Eris (Merck). Creatinine results were similar with both assays (Jaffe's reaction and enzymatic test) when measured in blood and urine. However the Jaffe's reaction gave higher creatinine results than the enzymatic test (p < 0.001), when assays were performed in peritoneal dialysis solutions and in pure glucose solutions. In addition, it appeared that other components of dialysis solutions, mainly calcium chloride, influenced unpredictably the results of creatinine with the Jaffe's reaction. We conclude that specific enzymatic test is a more accurate and reliable method to evaluate creatinine kinetics through the peritoneal membrane when determined in CAPD solutions.

Evaluation of ozone technology as an alternative for degradation of free gossypol in cottonseed meal: a prospective study

2021 ◽  
pp. 1-11
Author(s):  
Alessandra de Cássia Romero ◽  
Maria Antonia Calori-Domingues ◽  
Adibe Luiz Abdalla ◽  
Pedro Esteves Duarte Augusto
Keyword(s):  
Prospective Study ◽  
Cottonseed Meal ◽  
Free Gossypol ◽  
A Prospective Study

A Colorimetric Method for the Determination of Co-Ral in Animal Tissues1

1960 ◽  
Vol 53 (2) ◽  
pp. 263-265 ◽  
Author(s):  
H. V. Claborn ◽  
M. C. Ivey ◽  
H. D. Mann
Keyword(s):  
Colorimetric Method

Validation of a colorimetric method for determination of paracetamol in exhaled breath condensate

2021 ◽  
Author(s):  
Fariba Pourkarim ◽  
Elaheh Rahimpour ◽  
Maryam Khoubnasabjafari ◽  
Vahid Jouyban-Gharamaleki ◽  
Afshin Gharakhani ◽  
...  
Keyword(s):  
Exhaled Breath Condensate ◽  
Colorimetric Method ◽  
Exhaled Breath ◽  
Breath Condensate

Liquid Chromatographic Determination of Zoalene in Medicated Feeds

1984 ◽  
Vol 67 (5) ◽  
pp. 861-862 ◽  
Author(s):  
John Morawski ◽  
Glenn Kyle
Keyword(s):  
Colorimetric Method ◽  
Chromatographic Determination ◽  
Activated Alumina ◽  
Reverse Phase ◽  
Liquid Chromatographic Determination ◽  
Phase Liquid ◽  
Aoac Official ◽  
Liquid Chromatographic ◽  
Medicated Feeds

Abstract A rapid, reliable separation and quantitation of zoalene (3,5-dinitroo-toluamide) from feeds is accomplished by using reverse phase liquid chromatography (LC) and ultraviolet detection. An extraction technique which is similar to the present AOAC official colorimetric method is used before chromatographic analysis. This extraction is followed by an activated alumina cleanup and LC to separate zoalene from feed matrix. The methodology was applied to a variety of spiked feed matrices, and yielded good recoveries. Liquid chromatographic results were shown to correlate with colorimetric determinations.

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