Column Chromatography-Free Solution-Phase Synthesis of a Natural Piper-Amide-like Compound Library

2013 ◽  
Vol 15 (4) ◽  
pp. 208-215 ◽  
Author(s):  
Sumin Kim ◽  
Chaemin Lim ◽  
Sukjin Lee ◽  
Seokwoo Lee ◽  
Hyunkyung Cho ◽  
...  
Keyword(s):  
Column Chromatography ◽  
Solution Phase ◽  
Free Solution ◽  
Compound Library ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

scholarly journals The Synthesis of Two Combinatorial Libraries Using a 4-(2-Thienyl)-pyrrole Template

2002 ◽  
Vol 55 (12) ◽  
pp. 789 ◽  
Author(s):  
Rohan A. Davis ◽  
Anthony R. Carroll ◽  
Ronald J. Quinn
Keyword(s):  
Reductive Amination ◽  
Combinatorial Libraries ◽  
Solution Phase ◽  
Primary Amines ◽  
The Novel ◽  
Compound Library ◽  
Phase Synthesis ◽  
Parallel Solution ◽  
Tert Butyl ◽  
Solution Phase Synthesis

The synthesis of the novel biaryl compound, 4-(2-thienyl)-1H-pyrrole-2-carbaldehyde (1), by Suzuki–Miyaura coupling conditions is reported. Compound (1) was subsequently used as a combinatorial template in the parallel solution-phase synthesis of an amine and imine compound library. The amine library was produced using reductive amination conditions, and purification was achieved by a liquid–liquid partition followed by silica chromatography to afford ten amine analogues. The imine library consisted of five compounds, which were synthesized using volatile primary amines that allowed purification by evaporation. The synthesis of the novel and related biaryl carbaldehyde, tert-butyl-2-(5-formyl-1H-pyrrol-3-yl)-1H-pyrrole-1-carboxylate (2) is also reported.

Surfactant-free solution phase synthesis of monodispersed SnO2 hierarchical nanostructures and gas sensing properties

CrystEngComm ◽  
2012 ◽  
Vol 14 (9) ◽  
pp. 3169 ◽  
Author(s):  
Haijiao Zhang ◽  
Qingquan He ◽  
Xuedong Zhu ◽  
Dengyu Pan ◽  
Xiaoyong Deng ◽  
...  
Keyword(s):  
Gas Sensing ◽  
Solution Phase ◽  
Free Solution ◽  
Hierarchical Nanostructures ◽  
Phase Synthesis ◽  
Sensing Properties ◽  
Solution Phase Synthesis ◽  
Gas Sensing Properties

Ultrasmall Cu3N Nanoparticles: Surfactant-Free Solution-Phase Synthesis, Nitridation Mechanism, and Application for Lithium Storage

2015 ◽  
Vol 27 (24) ◽  
pp. 8282-8288 ◽  
Author(s):  
Rupali Deshmukh ◽  
Guobo Zeng ◽  
Elena Tervoort ◽  
Malwina Staniuk ◽  
David Wood ◽  
...  
Keyword(s):  
Solution Phase ◽  
Free Solution ◽  
Lithium Storage ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

Solution phase synthesis of oligonucleotides by the phosphoramidite method using solid supported reagents

2005 ◽  
Author(s):  
François Morvan ◽  
Aude-Emmanuelle Navarro ◽  
Cécile Dueymes ◽  
Ilaria Adamo ◽  
Andreas Schoenberger ◽  
...  
Keyword(s):  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

Polymer-Assisted Parallel Solution Phase Synthesis of Substituted Benzimidazoles.

ChemInform ◽  
2010 ◽  
Vol 33 (35) ◽  
pp. 123-123
Author(s):  
Young K. Yun ◽  
John A. Porco Jr. ◽  
Jeff Labadie
Keyword(s):  
Solution Phase ◽  
Phase Synthesis ◽  
Parallel Solution ◽  
Solution Phase Synthesis
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