Solid-Solution Nanoparticles:  Use of a Nonhydrolytic Sol−Gel Synthesis To Prepare HfO2and HfxZr1-xO2Nanocrystals

2004 ◽  
Vol 16 (7) ◽  
pp. 1336-1342 ◽  
Author(s):  
Jing Tang ◽  
Jason Fabbri ◽  
Richard D. Robinson ◽  
Yimei Zhu ◽  
Irving P. Herman ◽  
...  
Keyword(s):  
Solid Solution ◽  
Sol Gel ◽  
Sol Gel Synthesis

An Exafs Study of Compositional Homogeneity in Sol-gel Processed Potassium Tantalum Niobates

1998 ◽  
Vol 524 ◽  
Author(s):  
A. P. Wilkinson ◽  
J. XU ◽  
S. Pattanaik
Keyword(s):  
Solid Solution ◽  
Solid Solutions ◽  
Sol Gel ◽  
Direct Reaction ◽  
Sol Gel Process ◽  
Compositional Homogeneity ◽  
Exafs Study ◽  
Sol Gel Synthesis

ABSTRACTA series of K(Ta1-x Nbx)O3 solid-solution samples were prepared by direct reaction of oxides and carbonates, a homogeneous sol-gel process, and an inhomogeneous sol-gel process. The inhomogeneous sol-gel samples were prepared by the prehydrolysis of separate KTaO3 and KNbO3 precursor solutions followed by mixing of the resulting sols, drying and calcination. An examination of these samples by EXAFS at the Ta LIII and Nb K-edges, i) illustrated the difficulty of obtaining homogeneous solid solutions via direct reaction of oxides/carbonates, and ii) showed that the homogeneity of a solid-solution could be controlled by varying the hydrolysis procedure used during its sol-gel synthesis.

Sol–gel synthesis and structural characterisation of the perovskite type pseudo solid solution LaNi0.5Cu0.5O3

2002 ◽  
Vol 12 (5) ◽  
pp. 1370-1373 ◽  
Author(s):  
P. Odier ◽  
M. Municken ◽  
M. Crespin ◽  
F. Dubois ◽  
P. Mouron ◽  
...  
Keyword(s):  
Solid Solution ◽  
Sol Gel ◽  
Structural Characterisation ◽  
Sol Gel Synthesis ◽  
Perovskite Type

Inorganic-organic Hybrid Materials for Real 3-D Sub-νm Lithography

2003 ◽  
Vol 780 ◽  
Author(s):  
R. Houbertz ◽  
J. Schulz ◽  
L. Fröhlich ◽  
G. Domann ◽  
M. Popall ◽  
...  
Keyword(s):  
Femtosecond Laser ◽  
Sol Gel ◽  
Laser Pulses ◽  
Femtosecond Laser Pulses ◽  
Hybrid Polymer ◽  
Organic Hybrid ◽  
Two Photon ◽  
Applied Technology ◽  
Scale Structures ◽  
Sol Gel Synthesis

AbstractReal 3-D sub-νm lithography was performed with two-photon polymerization (2PP) using inorganic-organic hybrid polymer (ORMOCER®) resins. The hybrid polymers were synthesized by hydrolysis/polycondensation reactions (modified sol-gel synthesis) which allows one to tailor their material properties towards the respective applications, i.e., dielectrics, optics or passivation. Due to their photosensitive organic functionalities, ORMOCER®s can be patterned by conventional photo-lithography as well as by femtosecond laser pulses at 780 nm. This results in polymerized (solid) structures where the non-polymerized parts can be removed by conventional developers.ORMOCER® structures as small as 200 nm or even below were generated by 2PP of the resins using femtosecond laser pulses. It is demonstrated that ORMOCER®s have the potential to be used in components or devices built up by nm-scale structures such as, e.g., photonic crystals. Aspects of the materials in conjunction to the applied technology are discussed.

Sol-Gel Synthesis, Structure and Optical Properties of Nickel-Manganese Ferrites

2019 ◽  
Vol 11 (3) ◽  
pp. 03021-1-03021-5
Author(s):  
V. S. Bushkova ◽  
◽  
I. P. Yaremiy ◽  
B. K. Ostafiychuk ◽  
N. I. Riznychuk ◽  
...  
Keyword(s):  
Optical Properties ◽  
Sol Gel ◽  
Sol Gel Synthesis ◽  
Nickel Manganese

Sol-Gel Synthesis of Nano-Scale, End-Member Albite Feldspar (NaAlSi3O8)

2021 ◽  
Author(s):  
L.M. Anovitz ◽  
A. Affolter ◽  
M.C. Cheshire ◽  
A.J. Rondinone ◽  
Lawrence F. Allard
Keyword(s):  
Sol Gel ◽  
Nano Scale ◽  
Sol Gel Synthesis

scholarly journals Aqueous Sol-Gel Synthesis of Different Iron Ferrites: From 3D to 2D

Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1554
Author(s):  
Justinas Januskevicius ◽  
Zivile Stankeviciute ◽  
Dalis Baltrunas ◽  
Kęstutis Mažeika ◽  
Aldona Beganskiene ◽  
...  
Keyword(s):  
Magnetic Measurements ◽  
Substrate Surface ◽  
Sol Gel ◽  
Synthesis Method ◽  
Xrd Analysis ◽  
Dip Coating ◽  
Yttrium Iron ◽  
Iron Garnet ◽  
Dip Coating Technique ◽  
Sol Gel Synthesis

In this study, an aqueous sol-gel synthesis method and subsequent dip-coating technique were applied for the preparation of yttrium iron garnet (YIG), yttrium iron perovskite (YIP), and terbium iron perovskite (TIP) bulk and thin films. The monophasic highly crystalline different iron ferrite powders have been synthesized using this simple aqueous sol-gel process displaying the suitability of the method. In the next step, the same sol-gel solution was used for the fabrication of coatings on monocrystalline silicon (100) using a dip-coating procedure. This resulted, likely due to substrate surface influence, in all coatings having mixed phases of both garnet and perovskite. Thermogravimetric (TG) analysis of the precursor gels was carried out. All the samples were investigated by X-ray powder diffraction (XRD) analysis. The coatings were also investigated by scanning electron microscopy (SEM), atomic force microscopy (AFM) and Mössbauer spectroscopy. Magnetic measurements were also carried out.

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