Apatite Crystallization in an Aluminosilicate Glass Matrix:  Mechanistic Studies by X-ray Powder Diffraction, Thermal Analysis, and Multinuclear Solid-State NMR Spectroscopy

2001 ◽  
Vol 13 (11) ◽  
pp. 4198-4206 ◽  
Author(s):  
Jerry C. C. Chan ◽  
Richard Ohnsorge ◽  
Karin Meise-Gresch ◽  
Hellmut Eckert ◽  
Wolfram Höland ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
Glass Matrix ◽  
Aluminosilicate Glass ◽  
Mechanistic Studies ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

scholarly journals Synthesis, characterization and modeling of self-assembled porphyrin nanorods

2019 ◽  
Vol 23 (11n12) ◽  
pp. 1346-1354 ◽  
Author(s):  
Danielle Laurencin ◽  
Pascal G. Yot ◽  
Christel Gervais ◽  
Yannick Guari ◽  
Sébastien Clément ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dft Calculations ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
Molecular Level ◽  
Ion Association ◽  
Free Base ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

Porphyrin nanorods were prepared by ion-association between free-base meso 5,10,15,20-tetrakis-(4-[Formula: see text]-methylpyridinium)porphyrin cations and tetraphenylborate anions. The nanorods have variable lengths (up to a few micrometers long) and diameters ([Formula: see text]50–500 nm). Their structure at the molecular level was elucidated by combining multinuclear solid state NMR spectroscopy, synchrotron X-ray powder diffraction and DFT calculations.

Polypeptide Adsorption on a Synthetic Montmorillonite: A Combined Solid-State NMR Spectroscopy, X-ray Diffraction, Thermal Analysis and N2 Adsorption Study

2003 ◽  
Vol 2003 (7) ◽  
pp. 1366-1372 ◽  
Author(s):  
Régis D. Gougeon ◽  
Michel Soulard ◽  
Marc Reinholdt ◽  
Jocelyne Miehé-Brendlé ◽  
Jean-Michel Chézeau ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
X Ray Diffraction ◽  
N2 Adsorption ◽  
Adsorption Study ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

scholarly journals Probing the role of ceramide hydroxylation in skin barrier lipid models by 2H solid-state NMR spectroscopy and X-ray powder diffraction

2018 ◽  
Vol 1860 (5) ◽  
pp. 1162-1170 ◽  
Author(s):  
Andrej Kováčik ◽  
Alexander Vogel ◽  
Juliane Adler ◽  
Petra Pullmannová ◽  
Kateřina Vávrová ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
Skin Barrier ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

scholarly journals Structure of Tetrakis(melaminium) Bis(dihydrogenphosphate) Monohydrogenphosphate Trihydrate from X-ray Powder Diffraction and Solid-State NMR Spectroscopy

2008 ◽  
Vol 112 (32) ◽  
pp. 12515-12523 ◽  
Author(s):  
Vladimir Brodski ◽  
René Peschar ◽  
Henk Schenk ◽  
Andreas Brinkmann ◽  
Ernst R. H. van Eck ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

scholarly journals A New Methodological Approach to Correlate Protective and Microscopic Properties by Soft X-ray Microscopy and Solid State NMR Spectroscopy: The Case of Cusa’s Stone

2021 ◽  
Vol 11 (13) ◽  
pp. 5767
Author(s):  
Veronica Ciaramitaro ◽  
Alberto Spinella ◽  
Francesco Armetta ◽  
Roberto Scaffaro ◽  
Emmanuel Fortunato Gulino ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Methodological Approach ◽  
Polymer Chains ◽  
General Question ◽  
Protective Agent ◽  
Vapour Permeability ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

Hydrophobic treatment is one of the most important interventions usually carried out for the conservation of stone artefacts and monuments. The study here reported aims to answer a general question about how two polymers confer different protective performance. Two fluorinated-based polymer formulates applied on samples of Cusa’s stone confer a different level of water repellence and water vapour permeability. The observed protection action is here explained on the basis of chemico-physical interactions. The distribution of the polymer in the pore network was investigated using scanning electron microscopy and X-ray microscopy. The interactions between the stone substrate and the protective agents were investigated by means of solid state NMR spectroscopy. The ss-NMR findings reveal no significant changes in the chemical neighbourhood of the observed nuclei of each protective agent when applied onto the stone surface and provide information on the changes in the organization and dynamics of the studied systems, as well as on the mobility of polymer chains. This allowed us to explain the different macroscopic behaviours provided by each protective agent to the stone substrate.

scholarly journals Characterization and Quantitation of Clarithromycin Polymorphs by Powder X-Ray Diffractometry and Solid-State NMR Spectroscopy

2002 ◽  
Vol 50 (8) ◽  
pp. 1128-1130 ◽  
Author(s):  
Yuichi Tozuka ◽  
Atsutoshi Ito ◽  
Hiroko Seki ◽  
Toshio Oguchi ◽  
Keiji Yamamoto
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

Molecular structure and dynamics of C-1-adamantyl substituted N-unsubstituted pyrazoles studied by solid state NMR spectroscopy and X-ray crystallography

1997 ◽  
pp. 1867-1876 ◽  
Author(s):  
Rosa María Claramunt ◽  
María Dolores Santa María ◽  
Isabelle Forfar ◽  
Francisco Aguilar-Parrilla ◽  
María Minguet-Bonvehí ◽  
...  
Keyword(s):  
Molecular Structure ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
X Ray ◽  
Solid State Nmr Spectroscopy ◽  
X Ray Crystallography ◽  
Structure And Dynamics
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