Nucleation and Crystallization Kinetics of a Multicomponent Lithium Disilicate Glass by in Situ and Real-Time Synchrotron X-ray Diffraction

2013 ◽  
Vol 13 (9) ◽  
pp. 4031-4038 ◽  
Author(s):  
Saifang Huang ◽  
Peng Cao ◽  
Ying Li ◽  
Zhaohui Huang ◽  
Wei Gao
Keyword(s):  
Real Time ◽  
Crystallization Kinetics ◽  
Lithium Disilicate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Kinetics Of

Grain-Growth Kinetics of Nanocrystalline Iron Studied In Situ by Synchrotron Real-Time X-ray Diffraction

2000 ◽  
Vol 104 (11) ◽  
pp. 2467-2476 ◽  
Author(s):  
H. Natter ◽  
M. Schmelzer ◽  
M.-S Löffler ◽  
C. E. Krill ◽  
A. Fitch ◽  
...  
Keyword(s):  
Real Time ◽  
Grain Growth ◽  
Growth Kinetics ◽  
X Ray Diffraction ◽  
X Ray ◽  
Nanocrystalline Iron ◽  
Grain Growth Kinetics ◽  
Kinetics Of

scholarly journals In situ probing of the crystallization kinetics of rr-P3HT on single layer graphene as a function of temperature

2017 ◽  
Vol 19 (12) ◽  
pp. 8496-8503 ◽  
Author(s):  
Nicolas Boulanger ◽  
Victor Yu ◽  
Michael Hilke ◽  
Michael F. Toney ◽  
David R. Barbero
Keyword(s):  
Diffraction Analysis ◽  
Crystallization Kinetics ◽  
Single Layer ◽  
Single Layer Graphene ◽  
X Ray Diffraction ◽  
X Ray ◽  
Layer Graphene ◽  
Kinetics Of

In situ X-ray diffraction analysis of P3HT films during cooling down on both Si and G.

In-Situ X-ray Diffraction Study of the Crystallization Kinetics of Mesoporous Titania Films

2004 ◽  
Vol 108 (34) ◽  
pp. 12698-12706 ◽  
Author(s):  
Bradley L. Kirsch ◽  
Erik K. Richman ◽  
Andrew E. Riley ◽  
Sarah H. Tolbert
Keyword(s):  
Diffraction Study ◽  
Crystallization Kinetics ◽  
Mesoporous Titania ◽  
X Ray Diffraction ◽  
X Ray ◽  
Titania Films ◽  
Kinetics Of

scholarly journals In situ synchrotron radiation X-ray diffraction study of crystallization kinetics of polymorphs of 1,3-dioleoyl-2-palmitoyl glycerol (OPO)

CrystEngComm ◽  
2011 ◽  
Vol 13 (10) ◽  
pp. 3592 ◽  
Author(s):  
Laura Bayés-García ◽  
Teresa Calvet ◽  
Miquel Àngel Cuevas-Diarte ◽  
Satoru Ueno ◽  
Kiyotaka Sato
Keyword(s):  
Synchrotron Radiation ◽  
Diffraction Study ◽  
Crystallization Kinetics ◽  
X Ray Diffraction ◽  
X Ray ◽  
Palmitoyl Glycerol ◽  
Kinetics Of

Kinetics of Ion-Exchange Reactions in Hybrid Organic–Inorganic Perovskite Thin Films Studied by In Situ Real-Time X-ray Scattering

2018 ◽  
Vol 9 (23) ◽  
pp. 6750-6754 ◽  
Author(s):  
Alessandro Greco ◽  
Alexander Hinderhofer ◽  
M. Ibrahim Dar ◽  
Neha Arora ◽  
Jan Hagenlocher ◽  
...  
Keyword(s):  
Thin Films ◽  
Ion Exchange ◽  
Real Time ◽  
Exchange Reactions ◽  
Inorganic Perovskite ◽  
X Ray ◽  
X Ray Scattering ◽  
Kinetics Of ◽  
Kinetics Of Ion Exchange

scholarly journals In situ monitoring of hydrothermal reactions by X-ray diffraction with Bragg–Brentano geometry

2020 ◽  
Vol 53 (4) ◽  
pp. 1163-1166
Author(s):  
Karsten Mesecke ◽  
Winfried Malorny ◽  
Laurence N. Warr
Keyword(s):  
Quantitative Information ◽  
In Situ Monitoring ◽  
X Ray Diffraction ◽  
Hydrothermal Conditions ◽  
X Ray ◽  
Saturated Vapour Pressure ◽  
Concrete Production ◽  
Aerated Concrete ◽  
Kinetics Of

This note describes an autoclave chamber developed and constructed by Anton Paar and its application for in situ experiments under hydrothermal conditions. Reactions of crystalline phases can be studied by successive in situ measurements on a conventional laboratory X-ray diffractometer with Bragg–Brentano geometry at temperatures <483 K and saturated vapour pressure <2 MPa. Variations in the intensity of X-ray diffraction reflections of both reactants and products provide quantitative information for studying the reaction kinetics of both dissolution and crystal growth. Feasibility is demonstrated by studying a cementitious mixture used for autoclaved aerated concrete production. During a period of 5.7 h at 466 K and 1.35 MPa, the crystallization of torbermorite and the partial consumption of quartz were monitored.

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