HPLC/TOF-MS: An Alternative to LC/MS/MS for Sensitive and Selective Determination of Polar Organic Contaminants in the Aquatic Environment

2003 ◽  
pp. 109-127 ◽  
Author(s):  
M. J. Benotti ◽  
P. Lee Ferguson ◽  
R. A. Rieger ◽  
C. R. Iden ◽  
C. E. Heine ◽  
...  
Keyword(s):  
Organic Contaminants ◽  
Aquatic Environment ◽  
Selective Determination ◽  
Tof Ms

Chemical Fingerprinting and Multi-marker Determination of the Roots of Indigofera stachyoides by UHPLC-Q-TOF/MS

2015 ◽  
Vol 11 (4) ◽  
pp. 260-268 ◽  
Author(s):  
Ya-Xin Yang ◽  
Ai-Min Wang ◽  
Zheng Wang ◽  
Yong-Lin Wang ◽  
Jin Zhang ◽  
...  
Keyword(s):  
Chemical Fingerprinting ◽  
Tof Ms

Laser optoacoustic detection of trace concentration levels of ethylene, vinylchloride, and styrene in the atmosphere

1989 ◽  
Vol 54 (10) ◽  
pp. 2667-2673 ◽  
Author(s):  
Vojtěch Steiner ◽  
Pavel Engst ◽  
Zdeněk Zelinger ◽  
Milan Horák
Keyword(s):  
Detection Limit ◽  
Emission Line ◽  
Laser Line ◽  
Laser Source ◽  
Trace Concentration ◽  
Selective Determination ◽  
Hygienic Standard ◽  
Trace Concentrations ◽  
Concentration Levels

The optoacoustic analyzer with a tunable CO2 laser source employed in the present work permits a selective determination of ethylene in trace concentrations higher than 5 ppb (=detection limit for the 10P(14) emission line of the CO2 laser, ν = 949.5 cm-1) and of vinylchloride higher than 42 ppb (= detection limit for the 10P(22) CO2 laser line, ν= 942.4 cm-1). this method covers for both compounds the concentration range corresponding to the hygienic standard. It can be also used for the determination of styrene vapour with concentrations higher than 1.5 ppm.

Novel palladium(II) selective membrane electrode based on 4-[(5-mercapto-1,3,4-thiadiazol-2-ylimino)methyl]benzene-1,3-diol

2010 ◽  
Vol 75 (5) ◽  
pp. 563-575 ◽  
Author(s):  
Moslem Mohammadi ◽  
Mehdi Khodadadian ◽  
Mohammad K. Rofouei
Keyword(s):  
Limit Of Detection ◽  
Membrane Electrode ◽  
Aqueous Samples ◽  
Selective Determination ◽  
Poly Vinyl Chloride ◽  
Selective Membrane ◽  
Ph Range ◽  
Palladium Content ◽  
Methyl Benzene

A plasticized poly(vinyl chloride) membrane electrode based on 4-[(5-mercapto-1,3,4-thiadiazol-2-ylimino)methyl]benzene-1,3-diol (L) for highly selective determination of palladium(II) (in PdCl42– form) is developed. The electrode showed a good Nernstian response (29.6 ± 0.4 mV per decade) over a wide concentration range (3.1 × 10–7 to 1.0 × 10–2 mol l–1). The limit of detection was 1.5 × 10–7 mol l–1. The electrode has a response time of about 20 s, and it can be used for at least 2 months without observing any considerable deviation from Nernstian response. The proposed electrode could be used in the pH range of 2.5–5.5. The practical utility of the electrode has been demonstrated by its use for the estimation of palladium content in aqueous samples.

scholarly journals Expert System for Catalytic Titrimetry—Part 2: Determination of Monobasic Carboxylic Acids

1998 ◽  
Vol 81 (5) ◽  
pp. 1077-1086
Author(s):  
Biljana F Abramovic ◽  
Borislav K Abramovic ◽  
Ferenc F Gaál ◽  
Danilo M Obradovtc
Keyword(s):  
Expert System ◽  
Carboxylic Acids ◽  
Selective Determination

Abstract An expert system (ES) to solve the problem of choosing a catalytic titrimetric procedure for determining monobasic carboxylic acids is described. Carboxylic acids were divided into 3 groups—aliphatic, aromatic, and α-aminocarboxylic acids— based on their behavior in catalytic titrations with different indicator reactions, titrant, and/or solvent and the possibility of their selective determination in the presence of other acids

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